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Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification

Most organic solvents are colorless liquids, usually stored in sealed containers. In many cases, their identification depends on the appropriate description on the container to prevent mishandling or mixing with other materials. Although modern laboratories rely heavily on identification technologie...

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Detalles Bibliográficos
Autores principales: Rozman, Martin, Lukšič, Miha
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9780910/
https://www.ncbi.nlm.nih.gov/pubmed/36557555
http://dx.doi.org/10.3390/mi13122256
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author Rozman, Martin
Lukšič, Miha
author_facet Rozman, Martin
Lukšič, Miha
author_sort Rozman, Martin
collection PubMed
description Most organic solvents are colorless liquids, usually stored in sealed containers. In many cases, their identification depends on the appropriate description on the container to prevent mishandling or mixing with other materials. Although modern laboratories rely heavily on identification technologies, such as digitized inventories and spectroscopic methods (e.g., NMR or FTIR), there may be situations where these cannot be used due to technical failure, lack of equipment, or time. An example of a portable and cost-effective solution to this problem is an electrochemical sensor. However, these are often limited to electrochemical impedance spectroscopy (EIS) or voltammetry methods. To address this problem, we present a novel modular electrochemical sensor for solvent identification that can be used with either an EIS-enabled potentiostat/galvanostat or a simple multimeter. A novel method of fabricating and using a sensor consisting of a thin-film coating of an organic substance on a stainless-steel electrode substrate is presented. The differences in the solubility of the thin film in different solvents are used to distinguish between common organic solvents such as water, ethanol, and tetrahydrofuran.
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spelling pubmed-97809102022-12-24 Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification Rozman, Martin Lukšič, Miha Micromachines (Basel) Article Most organic solvents are colorless liquids, usually stored in sealed containers. In many cases, their identification depends on the appropriate description on the container to prevent mishandling or mixing with other materials. Although modern laboratories rely heavily on identification technologies, such as digitized inventories and spectroscopic methods (e.g., NMR or FTIR), there may be situations where these cannot be used due to technical failure, lack of equipment, or time. An example of a portable and cost-effective solution to this problem is an electrochemical sensor. However, these are often limited to electrochemical impedance spectroscopy (EIS) or voltammetry methods. To address this problem, we present a novel modular electrochemical sensor for solvent identification that can be used with either an EIS-enabled potentiostat/galvanostat or a simple multimeter. A novel method of fabricating and using a sensor consisting of a thin-film coating of an organic substance on a stainless-steel electrode substrate is presented. The differences in the solubility of the thin film in different solvents are used to distinguish between common organic solvents such as water, ethanol, and tetrahydrofuran. MDPI 2022-12-19 /pmc/articles/PMC9780910/ /pubmed/36557555 http://dx.doi.org/10.3390/mi13122256 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Rozman, Martin
Lukšič, Miha
Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification
title Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification
title_full Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification
title_fullStr Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification
title_full_unstemmed Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification
title_short Stainless Steel Foil-Based Label-Free Modular Thin-Film Electrochemical Detector for Solvent Identification
title_sort stainless steel foil-based label-free modular thin-film electrochemical detector for solvent identification
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9780910/
https://www.ncbi.nlm.nih.gov/pubmed/36557555
http://dx.doi.org/10.3390/mi13122256
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