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Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity

In this study, magnetite nanoparticles (Fe(3)O(4) NPs) were synthesized using Baccaurea ramiflora leaf extracts and characterized by visual observation, UV–Vis, FTIR, XRD, FESEM, and EDS. The UV−Vis spectrum showed continuous absorption at 300–500 nm, confirming the formation of Fe(3)O(4) NPs. FTIR...

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Autores principales: Khatun, Rokeya, Mamun, Muhammad Shamim Al, Islam, Suravi, Khatun, Nazia, Hakim, Mahmuda, Hossain, Muhammad Sarwar, Dhar, Palash Kumar, Barai, Hasi Rani
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9784331/
https://www.ncbi.nlm.nih.gov/pubmed/36557376
http://dx.doi.org/10.3390/mi13122077
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author Khatun, Rokeya
Mamun, Muhammad Shamim Al
Islam, Suravi
Khatun, Nazia
Hakim, Mahmuda
Hossain, Muhammad Sarwar
Dhar, Palash Kumar
Barai, Hasi Rani
author_facet Khatun, Rokeya
Mamun, Muhammad Shamim Al
Islam, Suravi
Khatun, Nazia
Hakim, Mahmuda
Hossain, Muhammad Sarwar
Dhar, Palash Kumar
Barai, Hasi Rani
author_sort Khatun, Rokeya
collection PubMed
description In this study, magnetite nanoparticles (Fe(3)O(4) NPs) were synthesized using Baccaurea ramiflora leaf extracts and characterized by visual observation, UV–Vis, FTIR, XRD, FESEM, and EDS. The UV−Vis spectrum showed continuous absorption at 300–500 nm, confirming the formation of Fe(3)O(4) NPs. FTIR revealed that compounds containing the O-H group act as reducing agents during Fe(3)O(4) NPs formation. Agglomerated spherical NPs were observed in the FESEM image. The prominent peak at ~6.4 keV in the EDS spectrum ascertained the existence of Fe, while the sharp peak at ~0.53 keV confirmed the presence of elemental oxygen. XRD patterns affirmed the crystalline nature. The size of as-synthesized NPs was observed to be 8.83 nm. The catalytic activity of Fe(3)O(4) NPs for the reduction of methylene blue (MB) dye was monitored by UV–Vis. The maximum absorption peak of MB dye at 664 nm was almost diminished within 20 min, which revealed Fe(3)O(4) NPs could be an excellent catalyst for wastewater treatment.
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spelling pubmed-97843312022-12-24 Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity Khatun, Rokeya Mamun, Muhammad Shamim Al Islam, Suravi Khatun, Nazia Hakim, Mahmuda Hossain, Muhammad Sarwar Dhar, Palash Kumar Barai, Hasi Rani Micromachines (Basel) Article In this study, magnetite nanoparticles (Fe(3)O(4) NPs) were synthesized using Baccaurea ramiflora leaf extracts and characterized by visual observation, UV–Vis, FTIR, XRD, FESEM, and EDS. The UV−Vis spectrum showed continuous absorption at 300–500 nm, confirming the formation of Fe(3)O(4) NPs. FTIR revealed that compounds containing the O-H group act as reducing agents during Fe(3)O(4) NPs formation. Agglomerated spherical NPs were observed in the FESEM image. The prominent peak at ~6.4 keV in the EDS spectrum ascertained the existence of Fe, while the sharp peak at ~0.53 keV confirmed the presence of elemental oxygen. XRD patterns affirmed the crystalline nature. The size of as-synthesized NPs was observed to be 8.83 nm. The catalytic activity of Fe(3)O(4) NPs for the reduction of methylene blue (MB) dye was monitored by UV–Vis. The maximum absorption peak of MB dye at 664 nm was almost diminished within 20 min, which revealed Fe(3)O(4) NPs could be an excellent catalyst for wastewater treatment. MDPI 2022-11-26 /pmc/articles/PMC9784331/ /pubmed/36557376 http://dx.doi.org/10.3390/mi13122077 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Khatun, Rokeya
Mamun, Muhammad Shamim Al
Islam, Suravi
Khatun, Nazia
Hakim, Mahmuda
Hossain, Muhammad Sarwar
Dhar, Palash Kumar
Barai, Hasi Rani
Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity
title Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity
title_full Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity
title_fullStr Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity
title_full_unstemmed Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity
title_short Phytochemical-Assisted Synthesis of Fe(3)O(4) Nanoparticles and Evaluation of Their Catalytic Activity
title_sort phytochemical-assisted synthesis of fe(3)o(4) nanoparticles and evaluation of their catalytic activity
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9784331/
https://www.ncbi.nlm.nih.gov/pubmed/36557376
http://dx.doi.org/10.3390/mi13122077
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