Cargando…
Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
New nanocomposites containing zirconium were synthesized using microwave irradiation. Their structure was confirmed by vibrating sample magnetometer (VSM) curves, X-ray diffraction (XRD) patterns, scanning electron microscope (SEM) and transmission electron microscopy (TEM) images, Fourier transform...
Autores principales: | , , , , , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9784536/ https://www.ncbi.nlm.nih.gov/pubmed/36558322 http://dx.doi.org/10.3390/nano12244468 |
_version_ | 1784857835626037248 |
---|---|
author | Asiri, Mohammed Abdulsalam, Ahmed Ghalib Kahtan, Mustafa Alsaikhan, Fahad Farhan, Issa Mutlak, Dhameer A. Hadrawi, Salema K. Suliman, Muath Di Lorenzo, Ritamaria Laneri, Sonia |
author_facet | Asiri, Mohammed Abdulsalam, Ahmed Ghalib Kahtan, Mustafa Alsaikhan, Fahad Farhan, Issa Mutlak, Dhameer A. Hadrawi, Salema K. Suliman, Muath Di Lorenzo, Ritamaria Laneri, Sonia |
author_sort | Asiri, Mohammed |
collection | PubMed |
description | New nanocomposites containing zirconium were synthesized using microwave irradiation. Their structure was confirmed by vibrating sample magnetometer (VSM) curves, X-ray diffraction (XRD) patterns, scanning electron microscope (SEM) and transmission electron microscopy (TEM) images, Fourier transform infrared spectroscopy (FT-IR), and Brunauer–Emmett–Teller (BET) N(2) adsorption/desorption isotherms. After the structure confirmation of the zirconium magnetic nanocomposite, the catalytic properties in the synthesis of pyrazole derivatives were investigated. Next, the biological activities of the zirconium magnetic nanocomposite, such as the antibacterial and antifungal activities, were investigated. The research results showed that the zirconium magnetic nanocomposite has high catalytic properties and can be used as a magnetic nanocatalyst for synthesizing heterocyclic compounds such as pyrazole derivatives in addition to having high biological properties. The unique properties of the nanoparticles can be attributed to their synthesis method and microwave radiation. |
format | Online Article Text |
id | pubmed-9784536 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-97845362022-12-24 Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives Asiri, Mohammed Abdulsalam, Ahmed Ghalib Kahtan, Mustafa Alsaikhan, Fahad Farhan, Issa Mutlak, Dhameer A. Hadrawi, Salema K. Suliman, Muath Di Lorenzo, Ritamaria Laneri, Sonia Nanomaterials (Basel) Article New nanocomposites containing zirconium were synthesized using microwave irradiation. Their structure was confirmed by vibrating sample magnetometer (VSM) curves, X-ray diffraction (XRD) patterns, scanning electron microscope (SEM) and transmission electron microscopy (TEM) images, Fourier transform infrared spectroscopy (FT-IR), and Brunauer–Emmett–Teller (BET) N(2) adsorption/desorption isotherms. After the structure confirmation of the zirconium magnetic nanocomposite, the catalytic properties in the synthesis of pyrazole derivatives were investigated. Next, the biological activities of the zirconium magnetic nanocomposite, such as the antibacterial and antifungal activities, were investigated. The research results showed that the zirconium magnetic nanocomposite has high catalytic properties and can be used as a magnetic nanocatalyst for synthesizing heterocyclic compounds such as pyrazole derivatives in addition to having high biological properties. The unique properties of the nanoparticles can be attributed to their synthesis method and microwave radiation. MDPI 2022-12-16 /pmc/articles/PMC9784536/ /pubmed/36558322 http://dx.doi.org/10.3390/nano12244468 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Asiri, Mohammed Abdulsalam, Ahmed Ghalib Kahtan, Mustafa Alsaikhan, Fahad Farhan, Issa Mutlak, Dhameer A. Hadrawi, Salema K. Suliman, Muath Di Lorenzo, Ritamaria Laneri, Sonia Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives |
title | Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives |
title_full | Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives |
title_fullStr | Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives |
title_full_unstemmed | Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives |
title_short | Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives |
title_sort | synthesis of new zirconium magnetic nanocomposite as a bioactive agent and green catalyst in the four-component synthesis of a novel multi-ring compound containing pyrazole derivatives |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9784536/ https://www.ncbi.nlm.nih.gov/pubmed/36558322 http://dx.doi.org/10.3390/nano12244468 |
work_keys_str_mv | AT asirimohammed synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT abdulsalamahmedghalib synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT kahtanmustafa synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT alsaikhanfahad synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT farhanissa synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT mutlakdhameera synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT hadrawisalemak synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT sulimanmuath synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT dilorenzoritamaria synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives AT lanerisonia synthesisofnewzirconiummagneticnanocompositeasabioactiveagentandgreencatalystinthefourcomponentsynthesisofanovelmultiringcompoundcontainingpyrazolederivatives |