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Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives

New nanocomposites containing zirconium were synthesized using microwave irradiation. Their structure was confirmed by vibrating sample magnetometer (VSM) curves, X-ray diffraction (XRD) patterns, scanning electron microscope (SEM) and transmission electron microscopy (TEM) images, Fourier transform...

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Autores principales: Asiri, Mohammed, Abdulsalam, Ahmed Ghalib, Kahtan, Mustafa, Alsaikhan, Fahad, Farhan, Issa, Mutlak, Dhameer A., Hadrawi, Salema K., Suliman, Muath, Di Lorenzo, Ritamaria, Laneri, Sonia
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9784536/
https://www.ncbi.nlm.nih.gov/pubmed/36558322
http://dx.doi.org/10.3390/nano12244468
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author Asiri, Mohammed
Abdulsalam, Ahmed Ghalib
Kahtan, Mustafa
Alsaikhan, Fahad
Farhan, Issa
Mutlak, Dhameer A.
Hadrawi, Salema K.
Suliman, Muath
Di Lorenzo, Ritamaria
Laneri, Sonia
author_facet Asiri, Mohammed
Abdulsalam, Ahmed Ghalib
Kahtan, Mustafa
Alsaikhan, Fahad
Farhan, Issa
Mutlak, Dhameer A.
Hadrawi, Salema K.
Suliman, Muath
Di Lorenzo, Ritamaria
Laneri, Sonia
author_sort Asiri, Mohammed
collection PubMed
description New nanocomposites containing zirconium were synthesized using microwave irradiation. Their structure was confirmed by vibrating sample magnetometer (VSM) curves, X-ray diffraction (XRD) patterns, scanning electron microscope (SEM) and transmission electron microscopy (TEM) images, Fourier transform infrared spectroscopy (FT-IR), and Brunauer–Emmett–Teller (BET) N(2) adsorption/desorption isotherms. After the structure confirmation of the zirconium magnetic nanocomposite, the catalytic properties in the synthesis of pyrazole derivatives were investigated. Next, the biological activities of the zirconium magnetic nanocomposite, such as the antibacterial and antifungal activities, were investigated. The research results showed that the zirconium magnetic nanocomposite has high catalytic properties and can be used as a magnetic nanocatalyst for synthesizing heterocyclic compounds such as pyrazole derivatives in addition to having high biological properties. The unique properties of the nanoparticles can be attributed to their synthesis method and microwave radiation.
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spelling pubmed-97845362022-12-24 Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives Asiri, Mohammed Abdulsalam, Ahmed Ghalib Kahtan, Mustafa Alsaikhan, Fahad Farhan, Issa Mutlak, Dhameer A. Hadrawi, Salema K. Suliman, Muath Di Lorenzo, Ritamaria Laneri, Sonia Nanomaterials (Basel) Article New nanocomposites containing zirconium were synthesized using microwave irradiation. Their structure was confirmed by vibrating sample magnetometer (VSM) curves, X-ray diffraction (XRD) patterns, scanning electron microscope (SEM) and transmission electron microscopy (TEM) images, Fourier transform infrared spectroscopy (FT-IR), and Brunauer–Emmett–Teller (BET) N(2) adsorption/desorption isotherms. After the structure confirmation of the zirconium magnetic nanocomposite, the catalytic properties in the synthesis of pyrazole derivatives were investigated. Next, the biological activities of the zirconium magnetic nanocomposite, such as the antibacterial and antifungal activities, were investigated. The research results showed that the zirconium magnetic nanocomposite has high catalytic properties and can be used as a magnetic nanocatalyst for synthesizing heterocyclic compounds such as pyrazole derivatives in addition to having high biological properties. The unique properties of the nanoparticles can be attributed to their synthesis method and microwave radiation. MDPI 2022-12-16 /pmc/articles/PMC9784536/ /pubmed/36558322 http://dx.doi.org/10.3390/nano12244468 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Asiri, Mohammed
Abdulsalam, Ahmed Ghalib
Kahtan, Mustafa
Alsaikhan, Fahad
Farhan, Issa
Mutlak, Dhameer A.
Hadrawi, Salema K.
Suliman, Muath
Di Lorenzo, Ritamaria
Laneri, Sonia
Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
title Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
title_full Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
title_fullStr Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
title_full_unstemmed Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
title_short Synthesis of New Zirconium Magnetic Nanocomposite as a Bioactive Agent and Green Catalyst in the Four-Component Synthesis of a Novel Multi-Ring Compound Containing Pyrazole Derivatives
title_sort synthesis of new zirconium magnetic nanocomposite as a bioactive agent and green catalyst in the four-component synthesis of a novel multi-ring compound containing pyrazole derivatives
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9784536/
https://www.ncbi.nlm.nih.gov/pubmed/36558322
http://dx.doi.org/10.3390/nano12244468
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