Cargando…

Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning

The cellulose of carex meyeriana kunth (CMKC) was used as raw material, and the spinning solution was prepared by combining with polyacrylonitrile (PAN). The nano-cellulose fiber of carex meyeriana kunth (CMKN) was prepared by electrospinning. Used to remove methylene blue dye (MB) in aqueous soluti...

Descripción completa

Detalles Bibliográficos
Autores principales: Sun, Ying, Yu, Yang, Li, Duanxin, Kong, Weishuai, Yang, Feng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9789126/
https://www.ncbi.nlm.nih.gov/pubmed/36564423
http://dx.doi.org/10.1038/s41598-022-25835-6
_version_ 1784858908231204864
author Sun, Ying
Yu, Yang
Li, Duanxin
Kong, Weishuai
Yang, Feng
author_facet Sun, Ying
Yu, Yang
Li, Duanxin
Kong, Weishuai
Yang, Feng
author_sort Sun, Ying
collection PubMed
description The cellulose of carex meyeriana kunth (CMKC) was used as raw material, and the spinning solution was prepared by combining with polyacrylonitrile (PAN). The nano-cellulose fiber of carex meyeriana kunth (CMKN) was prepared by electrospinning. Used to remove methylene blue dye (MB) in aqueous solution. In the electrospinning experiment, the addition of CMKC was in the range of 5% ~ 25%, the feed rate of spinning parameters was set in the range of 0.2 ~ 1.0 mL/h, the distance from the needle tip to the collecting plate was in the range of 10 ~ 25 cm, and the voltage was changed in the range of 15 ~ 25 kV. The obtained CMKN was characterized by scanning electron microscope, X-ray diffraction (XRD) and Fourier transform infrared spectroscopy. The MB removal rate was evaluated in the dye removal experiment, and the effects of CMKN on MB removal rate under the factors of CMKC dosage, temperature, shock time and MB initial concentration were discussed. The optimum process conditions were determined by response surface methodology. The results show that the prepared fibers are superfine fibers with nanometer diameter, and the spun nanofibers have smooth surface, high overall orientation and strong uniformity. The adsorption kinetics of prepared CMKN accords with quasi-second order model, and the adsorption isotherm accords with Langmuir model. The maximum dye removal rate of CMKN is 63.24%.
format Online
Article
Text
id pubmed-9789126
institution National Center for Biotechnology Information
language English
publishDate 2022
publisher Nature Publishing Group UK
record_format MEDLINE/PubMed
spelling pubmed-97891262022-12-25 Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning Sun, Ying Yu, Yang Li, Duanxin Kong, Weishuai Yang, Feng Sci Rep Article The cellulose of carex meyeriana kunth (CMKC) was used as raw material, and the spinning solution was prepared by combining with polyacrylonitrile (PAN). The nano-cellulose fiber of carex meyeriana kunth (CMKN) was prepared by electrospinning. Used to remove methylene blue dye (MB) in aqueous solution. In the electrospinning experiment, the addition of CMKC was in the range of 5% ~ 25%, the feed rate of spinning parameters was set in the range of 0.2 ~ 1.0 mL/h, the distance from the needle tip to the collecting plate was in the range of 10 ~ 25 cm, and the voltage was changed in the range of 15 ~ 25 kV. The obtained CMKN was characterized by scanning electron microscope, X-ray diffraction (XRD) and Fourier transform infrared spectroscopy. The MB removal rate was evaluated in the dye removal experiment, and the effects of CMKN on MB removal rate under the factors of CMKC dosage, temperature, shock time and MB initial concentration were discussed. The optimum process conditions were determined by response surface methodology. The results show that the prepared fibers are superfine fibers with nanometer diameter, and the spun nanofibers have smooth surface, high overall orientation and strong uniformity. The adsorption kinetics of prepared CMKN accords with quasi-second order model, and the adsorption isotherm accords with Langmuir model. The maximum dye removal rate of CMKN is 63.24%. Nature Publishing Group UK 2022-12-23 /pmc/articles/PMC9789126/ /pubmed/36564423 http://dx.doi.org/10.1038/s41598-022-25835-6 Text en © The Author(s) 2022 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Sun, Ying
Yu, Yang
Li, Duanxin
Kong, Weishuai
Yang, Feng
Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning
title Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning
title_full Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning
title_fullStr Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning
title_full_unstemmed Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning
title_short Preparation and characterization of carex meyeriana Kunthcellulose nanofibers by electrospinning
title_sort preparation and characterization of carex meyeriana kunthcellulose nanofibers by electrospinning
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9789126/
https://www.ncbi.nlm.nih.gov/pubmed/36564423
http://dx.doi.org/10.1038/s41598-022-25835-6
work_keys_str_mv AT sunying preparationandcharacterizationofcarexmeyerianakunthcellulosenanofibersbyelectrospinning
AT yuyang preparationandcharacterizationofcarexmeyerianakunthcellulosenanofibersbyelectrospinning
AT liduanxin preparationandcharacterizationofcarexmeyerianakunthcellulosenanofibersbyelectrospinning
AT kongweishuai preparationandcharacterizationofcarexmeyerianakunthcellulosenanofibersbyelectrospinning
AT yangfeng preparationandcharacterizationofcarexmeyerianakunthcellulosenanofibersbyelectrospinning