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Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
OBJECTIVE: This investigation evaluated the effect of two sintering modes of a translucent zirconia (Y‐TZP) on its surface roughness, topography, phase‐transformation (t → m), translucency and biaxial flexure fatigue strength. MATERIALS AND METHODS: To do so, 50 Y‐TZP discs (Ø = 15 mm; thickness = 1...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
John Wiley & Sons, Inc.
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9790507/ https://www.ncbi.nlm.nih.gov/pubmed/35560703 http://dx.doi.org/10.1111/jerd.12923 |
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author | Madruga, Camila Ferreira Leite Dal Piva, Amanda Maria de Oliveira Pereira, Gabriel Kalil Rocha Caneppele, Taciana Marco Ferraz Valandro, Luiz Felipe Bottino, Marco Antonio |
author_facet | Madruga, Camila Ferreira Leite Dal Piva, Amanda Maria de Oliveira Pereira, Gabriel Kalil Rocha Caneppele, Taciana Marco Ferraz Valandro, Luiz Felipe Bottino, Marco Antonio |
author_sort | Madruga, Camila Ferreira Leite |
collection | PubMed |
description | OBJECTIVE: This investigation evaluated the effect of two sintering modes of a translucent zirconia (Y‐TZP) on its surface roughness, topography, phase‐transformation (t → m), translucency and biaxial flexure fatigue strength. MATERIALS AND METHODS: To do so, 50 Y‐TZP discs (Ø = 15 mm; thickness = 1.2 mm; IPS e.max ZirCAD LT) were prepared and divided into two groups: Standard mode (SM) and Fast mode (FM). Staircase fatigue testing was performed (piston‐on‐three balls set‐up, ISO 6872:2015), as well as surface roughness, profilometry, scanning electron microscopy (SEM‐FEG), energy dispersive X‐ray spectroscopy (EDX), phase transformation (t → m) using X‐ray diffraction analysis (XRD), translucency parameter analysis (TP and TP(00)) and fractography. RESULTS: The results showed no statistical significant differences for roughness parameters (p > 0.05, SM: Ra = 0.13 ± 0.02, Rz = 1.21 ± 0.26 and RSm = 24.91 ± 2.19; FM: Ra = 0.14 ± 0.03, Rz = 1.32 ± 0.25 and RSm = 24.68 ± 2.16) or flexural fatigue strength (SM: 512 (464–560) MPa; FM: 542 (472–611) MPa) between the groups. In addition, similarity in surface morphological features (SEM and profilometry), composition and phases (EDX and XRD) was observed between the firing protocols. Fractography showed that the failure origin occurred on the tensile side. Sintering mode did not affect the TP (F = 0.001, p = 0.97) and TP(00) (F = 0.12, p = 0.72). CONCLUSIONS: Therefore, the fast‐sintering mode is suggested as a viable alternative to the standard mode since it does not influence the evaluated surface morphology, microstructure, fatigue strength and translucency of a translucent monolithic zirconia. CLINICAL SIGNIFICANCE: The fast sintering mode is a viable alternative for zirconia without compromising its topography, microstructure, mechanical performance or translucency. |
format | Online Article Text |
id | pubmed-9790507 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | John Wiley & Sons, Inc. |
record_format | MEDLINE/PubMed |
spelling | pubmed-97905072022-12-28 Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency Madruga, Camila Ferreira Leite Dal Piva, Amanda Maria de Oliveira Pereira, Gabriel Kalil Rocha Caneppele, Taciana Marco Ferraz Valandro, Luiz Felipe Bottino, Marco Antonio J Esthet Restor Dent Research Articles OBJECTIVE: This investigation evaluated the effect of two sintering modes of a translucent zirconia (Y‐TZP) on its surface roughness, topography, phase‐transformation (t → m), translucency and biaxial flexure fatigue strength. MATERIALS AND METHODS: To do so, 50 Y‐TZP discs (Ø = 15 mm; thickness = 1.2 mm; IPS e.max ZirCAD LT) were prepared and divided into two groups: Standard mode (SM) and Fast mode (FM). Staircase fatigue testing was performed (piston‐on‐three balls set‐up, ISO 6872:2015), as well as surface roughness, profilometry, scanning electron microscopy (SEM‐FEG), energy dispersive X‐ray spectroscopy (EDX), phase transformation (t → m) using X‐ray diffraction analysis (XRD), translucency parameter analysis (TP and TP(00)) and fractography. RESULTS: The results showed no statistical significant differences for roughness parameters (p > 0.05, SM: Ra = 0.13 ± 0.02, Rz = 1.21 ± 0.26 and RSm = 24.91 ± 2.19; FM: Ra = 0.14 ± 0.03, Rz = 1.32 ± 0.25 and RSm = 24.68 ± 2.16) or flexural fatigue strength (SM: 512 (464–560) MPa; FM: 542 (472–611) MPa) between the groups. In addition, similarity in surface morphological features (SEM and profilometry), composition and phases (EDX and XRD) was observed between the firing protocols. Fractography showed that the failure origin occurred on the tensile side. Sintering mode did not affect the TP (F = 0.001, p = 0.97) and TP(00) (F = 0.12, p = 0.72). CONCLUSIONS: Therefore, the fast‐sintering mode is suggested as a viable alternative to the standard mode since it does not influence the evaluated surface morphology, microstructure, fatigue strength and translucency of a translucent monolithic zirconia. CLINICAL SIGNIFICANCE: The fast sintering mode is a viable alternative for zirconia without compromising its topography, microstructure, mechanical performance or translucency. John Wiley & Sons, Inc. 2022-05-13 2022-12 /pmc/articles/PMC9790507/ /pubmed/35560703 http://dx.doi.org/10.1111/jerd.12923 Text en © 2022 The Authors. Journal of Esthetic and Restorative Dentistry published by Wiley Periodicals LLC. https://creativecommons.org/licenses/by-nc/4.0/This is an open access article under the terms of the http://creativecommons.org/licenses/by-nc/4.0/ (https://creativecommons.org/licenses/by-nc/4.0/) License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes. |
spellingShingle | Research Articles Madruga, Camila Ferreira Leite Dal Piva, Amanda Maria de Oliveira Pereira, Gabriel Kalil Rocha Caneppele, Taciana Marco Ferraz Valandro, Luiz Felipe Bottino, Marco Antonio Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency |
title | Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency |
title_full | Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency |
title_fullStr | Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency |
title_full_unstemmed | Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency |
title_short | Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency |
title_sort | sintering mode of a translucent y‐tzp: effects on its biaxial flexure fatigue strength, surface morphology and translucency |
topic | Research Articles |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9790507/ https://www.ncbi.nlm.nih.gov/pubmed/35560703 http://dx.doi.org/10.1111/jerd.12923 |
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