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Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency

OBJECTIVE: This investigation evaluated the effect of two sintering modes of a translucent zirconia (Y‐TZP) on its surface roughness, topography, phase‐transformation (t → m), translucency and biaxial flexure fatigue strength. MATERIALS AND METHODS: To do so, 50 Y‐TZP discs (Ø = 15 mm; thickness = 1...

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Autores principales: Madruga, Camila Ferreira Leite, Dal Piva, Amanda Maria de Oliveira, Pereira, Gabriel Kalil Rocha, Caneppele, Taciana Marco Ferraz, Valandro, Luiz Felipe, Bottino, Marco Antonio
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley & Sons, Inc. 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9790507/
https://www.ncbi.nlm.nih.gov/pubmed/35560703
http://dx.doi.org/10.1111/jerd.12923
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author Madruga, Camila Ferreira Leite
Dal Piva, Amanda Maria de Oliveira
Pereira, Gabriel Kalil Rocha
Caneppele, Taciana Marco Ferraz
Valandro, Luiz Felipe
Bottino, Marco Antonio
author_facet Madruga, Camila Ferreira Leite
Dal Piva, Amanda Maria de Oliveira
Pereira, Gabriel Kalil Rocha
Caneppele, Taciana Marco Ferraz
Valandro, Luiz Felipe
Bottino, Marco Antonio
author_sort Madruga, Camila Ferreira Leite
collection PubMed
description OBJECTIVE: This investigation evaluated the effect of two sintering modes of a translucent zirconia (Y‐TZP) on its surface roughness, topography, phase‐transformation (t → m), translucency and biaxial flexure fatigue strength. MATERIALS AND METHODS: To do so, 50 Y‐TZP discs (Ø = 15 mm; thickness = 1.2 mm; IPS e.max ZirCAD LT) were prepared and divided into two groups: Standard mode (SM) and Fast mode (FM). Staircase fatigue testing was performed (piston‐on‐three balls set‐up, ISO 6872:2015), as well as surface roughness, profilometry, scanning electron microscopy (SEM‐FEG), energy dispersive X‐ray spectroscopy (EDX), phase transformation (t → m) using X‐ray diffraction analysis (XRD), translucency parameter analysis (TP and TP(00)) and fractography. RESULTS: The results showed no statistical significant differences for roughness parameters (p > 0.05, SM: Ra = 0.13 ± 0.02, Rz = 1.21 ± 0.26 and RSm = 24.91 ± 2.19; FM: Ra = 0.14 ± 0.03, Rz = 1.32 ± 0.25 and RSm = 24.68 ± 2.16) or flexural fatigue strength (SM: 512 (464–560) MPa; FM: 542 (472–611) MPa) between the groups. In addition, similarity in surface morphological features (SEM and profilometry), composition and phases (EDX and XRD) was observed between the firing protocols. Fractography showed that the failure origin occurred on the tensile side. Sintering mode did not affect the TP (F = 0.001, p = 0.97) and TP(00) (F = 0.12, p = 0.72). CONCLUSIONS: Therefore, the fast‐sintering mode is suggested as a viable alternative to the standard mode since it does not influence the evaluated surface morphology, microstructure, fatigue strength and translucency of a translucent monolithic zirconia. CLINICAL SIGNIFICANCE: The fast sintering mode is a viable alternative for zirconia without compromising its topography, microstructure, mechanical performance or translucency.
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spelling pubmed-97905072022-12-28 Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency Madruga, Camila Ferreira Leite Dal Piva, Amanda Maria de Oliveira Pereira, Gabriel Kalil Rocha Caneppele, Taciana Marco Ferraz Valandro, Luiz Felipe Bottino, Marco Antonio J Esthet Restor Dent Research Articles OBJECTIVE: This investigation evaluated the effect of two sintering modes of a translucent zirconia (Y‐TZP) on its surface roughness, topography, phase‐transformation (t → m), translucency and biaxial flexure fatigue strength. MATERIALS AND METHODS: To do so, 50 Y‐TZP discs (Ø = 15 mm; thickness = 1.2 mm; IPS e.max ZirCAD LT) were prepared and divided into two groups: Standard mode (SM) and Fast mode (FM). Staircase fatigue testing was performed (piston‐on‐three balls set‐up, ISO 6872:2015), as well as surface roughness, profilometry, scanning electron microscopy (SEM‐FEG), energy dispersive X‐ray spectroscopy (EDX), phase transformation (t → m) using X‐ray diffraction analysis (XRD), translucency parameter analysis (TP and TP(00)) and fractography. RESULTS: The results showed no statistical significant differences for roughness parameters (p > 0.05, SM: Ra = 0.13 ± 0.02, Rz = 1.21 ± 0.26 and RSm = 24.91 ± 2.19; FM: Ra = 0.14 ± 0.03, Rz = 1.32 ± 0.25 and RSm = 24.68 ± 2.16) or flexural fatigue strength (SM: 512 (464–560) MPa; FM: 542 (472–611) MPa) between the groups. In addition, similarity in surface morphological features (SEM and profilometry), composition and phases (EDX and XRD) was observed between the firing protocols. Fractography showed that the failure origin occurred on the tensile side. Sintering mode did not affect the TP (F = 0.001, p = 0.97) and TP(00) (F = 0.12, p = 0.72). CONCLUSIONS: Therefore, the fast‐sintering mode is suggested as a viable alternative to the standard mode since it does not influence the evaluated surface morphology, microstructure, fatigue strength and translucency of a translucent monolithic zirconia. CLINICAL SIGNIFICANCE: The fast sintering mode is a viable alternative for zirconia without compromising its topography, microstructure, mechanical performance or translucency. John Wiley & Sons, Inc. 2022-05-13 2022-12 /pmc/articles/PMC9790507/ /pubmed/35560703 http://dx.doi.org/10.1111/jerd.12923 Text en © 2022 The Authors. Journal of Esthetic and Restorative Dentistry published by Wiley Periodicals LLC. https://creativecommons.org/licenses/by-nc/4.0/This is an open access article under the terms of the http://creativecommons.org/licenses/by-nc/4.0/ (https://creativecommons.org/licenses/by-nc/4.0/) License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited and is not used for commercial purposes.
spellingShingle Research Articles
Madruga, Camila Ferreira Leite
Dal Piva, Amanda Maria de Oliveira
Pereira, Gabriel Kalil Rocha
Caneppele, Taciana Marco Ferraz
Valandro, Luiz Felipe
Bottino, Marco Antonio
Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
title Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
title_full Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
title_fullStr Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
title_full_unstemmed Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
title_short Sintering mode of a translucent Y‐TZP: Effects on its biaxial flexure fatigue strength, surface morphology and translucency
title_sort sintering mode of a translucent y‐tzp: effects on its biaxial flexure fatigue strength, surface morphology and translucency
topic Research Articles
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9790507/
https://www.ncbi.nlm.nih.gov/pubmed/35560703
http://dx.doi.org/10.1111/jerd.12923
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