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Aerosol-assisted CVD method for the synthesis of solid particles of t-YSZ-Fe(3)O(4)
This work details the production of solid composite particles by the aerosol-assisted chemical vapor deposition method. With this method it is feasible to produce at low temperature (450 °C) the tetragonal phase of zirconium oxide stabilizing it with yttrium oxide (YSZ) and cubic iron oxide (Fe(3)O(...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9801192/ https://www.ncbi.nlm.nih.gov/pubmed/36590319 http://dx.doi.org/10.1016/j.mex.2022.101973 |
Sumario: | This work details the production of solid composite particles by the aerosol-assisted chemical vapor deposition method. With this method it is feasible to produce at low temperature (450 °C) the tetragonal phase of zirconium oxide stabilizing it with yttrium oxide (YSZ) and cubic iron oxide (Fe(3)O(4)) at the same time. The particles have a solid morphology in which both metal oxides coexist without mixing. The average size of the obtained particles is 329 ± 81 nm, moreover, each particle is formed by thousands of crystallites of size 2 ± 0.5 nm. The formation of solid structures is due to the amount of Zr and Y found in each particle. These particles can be applied as reinforcements of metallic structures. • A simple and low-cost method for producing composite particles to be applied as reinforcing agents for metal structures. • The particles are formed by two phases of tetragonal yttria-stabilized zirconia (t-YSZ) and cubic Fe(3)O(4), which was synthesized following a one-step process via the aerosol-assisted chemical vapor deposition method (AACVD). • The tetragonal phase of ZrO(2) is obtained at 450 °C stabilizing it with ∼3.8% of yttrium oxide. |
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