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Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
The one-pot synthesis process has emerged as an economical synthesis method without the involvement of purification or formation of intermediate compounds. Therefore, nickel nanoparticles were selectively synthesized by a simple hydrothermal method using nickel(II) chloride hexahydrate and borane–am...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2022
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9821542/ https://www.ncbi.nlm.nih.gov/pubmed/36614416 http://dx.doi.org/10.3390/ma16010076 |
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author | Kim, Gawon Na, Chan Woong Myung, Yoon |
author_facet | Kim, Gawon Na, Chan Woong Myung, Yoon |
author_sort | Kim, Gawon |
collection | PubMed |
description | The one-pot synthesis process has emerged as an economical synthesis method without the involvement of purification or formation of intermediate compounds. Therefore, nickel nanoparticles were selectively synthesized by a simple hydrothermal method using nickel(II) chloride hexahydrate and borane–ammonia complex as a precursor and reducing agent, respectively. The morphology and crystal growth were observed by controlling the precursor concentration ratio of Ni:AB from 1:0.1 to 1:4 under various temperatures ranging from 80 to 140 degrees. In addition, we observed that the crystal growth rate under the influence of NaCl and KCl resulted in spherical Ni particles with size distributions controlled in the range of 297.65 nm to 1082.15 nm and 358.6 nm to 605 nm, respectively. |
format | Online Article Text |
id | pubmed-9821542 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2022 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-98215422023-01-07 Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method Kim, Gawon Na, Chan Woong Myung, Yoon Materials (Basel) Article The one-pot synthesis process has emerged as an economical synthesis method without the involvement of purification or formation of intermediate compounds. Therefore, nickel nanoparticles were selectively synthesized by a simple hydrothermal method using nickel(II) chloride hexahydrate and borane–ammonia complex as a precursor and reducing agent, respectively. The morphology and crystal growth were observed by controlling the precursor concentration ratio of Ni:AB from 1:0.1 to 1:4 under various temperatures ranging from 80 to 140 degrees. In addition, we observed that the crystal growth rate under the influence of NaCl and KCl resulted in spherical Ni particles with size distributions controlled in the range of 297.65 nm to 1082.15 nm and 358.6 nm to 605 nm, respectively. MDPI 2022-12-21 /pmc/articles/PMC9821542/ /pubmed/36614416 http://dx.doi.org/10.3390/ma16010076 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Kim, Gawon Na, Chan Woong Myung, Yoon Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method |
title | Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method |
title_full | Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method |
title_fullStr | Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method |
title_full_unstemmed | Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method |
title_short | Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method |
title_sort | facile one-pot synthesis of nickel nanoparticles by hydrothermal method |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9821542/ https://www.ncbi.nlm.nih.gov/pubmed/36614416 http://dx.doi.org/10.3390/ma16010076 |
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