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Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method

The one-pot synthesis process has emerged as an economical synthesis method without the involvement of purification or formation of intermediate compounds. Therefore, nickel nanoparticles were selectively synthesized by a simple hydrothermal method using nickel(II) chloride hexahydrate and borane–am...

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Detalles Bibliográficos
Autores principales: Kim, Gawon, Na, Chan Woong, Myung, Yoon
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2022
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9821542/
https://www.ncbi.nlm.nih.gov/pubmed/36614416
http://dx.doi.org/10.3390/ma16010076
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author Kim, Gawon
Na, Chan Woong
Myung, Yoon
author_facet Kim, Gawon
Na, Chan Woong
Myung, Yoon
author_sort Kim, Gawon
collection PubMed
description The one-pot synthesis process has emerged as an economical synthesis method without the involvement of purification or formation of intermediate compounds. Therefore, nickel nanoparticles were selectively synthesized by a simple hydrothermal method using nickel(II) chloride hexahydrate and borane–ammonia complex as a precursor and reducing agent, respectively. The morphology and crystal growth were observed by controlling the precursor concentration ratio of Ni:AB from 1:0.1 to 1:4 under various temperatures ranging from 80 to 140 degrees. In addition, we observed that the crystal growth rate under the influence of NaCl and KCl resulted in spherical Ni particles with size distributions controlled in the range of 297.65 nm to 1082.15 nm and 358.6 nm to 605 nm, respectively.
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spelling pubmed-98215422023-01-07 Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method Kim, Gawon Na, Chan Woong Myung, Yoon Materials (Basel) Article The one-pot synthesis process has emerged as an economical synthesis method without the involvement of purification or formation of intermediate compounds. Therefore, nickel nanoparticles were selectively synthesized by a simple hydrothermal method using nickel(II) chloride hexahydrate and borane–ammonia complex as a precursor and reducing agent, respectively. The morphology and crystal growth were observed by controlling the precursor concentration ratio of Ni:AB from 1:0.1 to 1:4 under various temperatures ranging from 80 to 140 degrees. In addition, we observed that the crystal growth rate under the influence of NaCl and KCl resulted in spherical Ni particles with size distributions controlled in the range of 297.65 nm to 1082.15 nm and 358.6 nm to 605 nm, respectively. MDPI 2022-12-21 /pmc/articles/PMC9821542/ /pubmed/36614416 http://dx.doi.org/10.3390/ma16010076 Text en © 2022 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kim, Gawon
Na, Chan Woong
Myung, Yoon
Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
title Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
title_full Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
title_fullStr Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
title_full_unstemmed Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
title_short Facile One-Pot Synthesis of Nickel Nanoparticles by Hydrothermal Method
title_sort facile one-pot synthesis of nickel nanoparticles by hydrothermal method
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9821542/
https://www.ncbi.nlm.nih.gov/pubmed/36614416
http://dx.doi.org/10.3390/ma16010076
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