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Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy

In this study, the as-cast microstructure and the evolution of the homogenized microstructure of large-scale industrialized Al-Cu-Mg-Ag heat-resistant aluminum alloy ingots were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive analysis (EDS), an...

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Autores principales: Lin, Haitao, Zhu, Kai, Liu, Qilong, Chen, Lifang, Wang, Zhengan, Li, Xiwu
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9822060/
https://www.ncbi.nlm.nih.gov/pubmed/36614772
http://dx.doi.org/10.3390/ma16010433
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author Lin, Haitao
Zhu, Kai
Liu, Qilong
Chen, Lifang
Wang, Zhengan
Li, Xiwu
author_facet Lin, Haitao
Zhu, Kai
Liu, Qilong
Chen, Lifang
Wang, Zhengan
Li, Xiwu
author_sort Lin, Haitao
collection PubMed
description In this study, the as-cast microstructure and the evolution of the homogenized microstructure of large-scale industrialized Al-Cu-Mg-Ag heat-resistant aluminum alloy ingots were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive analysis (EDS), and differential scanning calorimetry (DSC). The results indicate that the dendritic segregation is evident in the ingot along the radial direction, and the grain boundaries are decorated with lots of net-shaped continuous eutectic structures. With the homogenization time extension and the homogenization temperature increase, the eutectic phases (i.e., the primary Al(2)Cu phase, the Al(2)CuMg phase, and the AlCuMgAg quaternary phase) at the grain boundaries gradually dissolve back into the matrix. Meanwhile, most of the dendritic grain boundaries gradually become sparse and thinner. Finally, it is found that the optimal homogenization regime of the Al-Cu-Mg-Ag alloy is 420 °C/5 h+480 °C/8 h+515 °C/24 h.
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spelling pubmed-98220602023-01-07 Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy Lin, Haitao Zhu, Kai Liu, Qilong Chen, Lifang Wang, Zhengan Li, Xiwu Materials (Basel) Article In this study, the as-cast microstructure and the evolution of the homogenized microstructure of large-scale industrialized Al-Cu-Mg-Ag heat-resistant aluminum alloy ingots were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive analysis (EDS), and differential scanning calorimetry (DSC). The results indicate that the dendritic segregation is evident in the ingot along the radial direction, and the grain boundaries are decorated with lots of net-shaped continuous eutectic structures. With the homogenization time extension and the homogenization temperature increase, the eutectic phases (i.e., the primary Al(2)Cu phase, the Al(2)CuMg phase, and the AlCuMgAg quaternary phase) at the grain boundaries gradually dissolve back into the matrix. Meanwhile, most of the dendritic grain boundaries gradually become sparse and thinner. Finally, it is found that the optimal homogenization regime of the Al-Cu-Mg-Ag alloy is 420 °C/5 h+480 °C/8 h+515 °C/24 h. MDPI 2023-01-03 /pmc/articles/PMC9822060/ /pubmed/36614772 http://dx.doi.org/10.3390/ma16010433 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Lin, Haitao
Zhu, Kai
Liu, Qilong
Chen, Lifang
Wang, Zhengan
Li, Xiwu
Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy
title Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy
title_full Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy
title_fullStr Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy
title_full_unstemmed Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy
title_short Microstructural Characterization of the As-Cast and Homogenized Al-Cu-Mg-Ag Alloy
title_sort microstructural characterization of the as-cast and homogenized al-cu-mg-ag alloy
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9822060/
https://www.ncbi.nlm.nih.gov/pubmed/36614772
http://dx.doi.org/10.3390/ma16010433
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