Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst

[Image: see text] The Schiff bases were prepared with aromatic aldehyde and aromatic amine using cashew shell extract as a catalyst under microwave irradiation. This reaction is rapid, efficient, and solvent-free and involves the one-pot synthesis of Schiff bases under microwave irradiation. The syn...

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Autores principales: Manjare, Satish B., Mahadik, Rakesh K., Manval, Kalpesh S., More, Prajal P., Dalvi, Siddhesh S.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2022
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9835518/
https://www.ncbi.nlm.nih.gov/pubmed/36643449
http://dx.doi.org/10.1021/acsomega.2c05187
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author Manjare, Satish B.
Mahadik, Rakesh K.
Manval, Kalpesh S.
More, Prajal P.
Dalvi, Siddhesh S.
author_facet Manjare, Satish B.
Mahadik, Rakesh K.
Manval, Kalpesh S.
More, Prajal P.
Dalvi, Siddhesh S.
author_sort Manjare, Satish B.
collection PubMed
description [Image: see text] The Schiff bases were prepared with aromatic aldehyde and aromatic amine using cashew shell extract as a catalyst under microwave irradiation. This reaction is rapid, efficient, and solvent-free and involves the one-pot synthesis of Schiff bases under microwave irradiation. The synthesized Schiff bases were characterized by Fourier transform infrared (FTIR) spectroscopy, (1)H nuclear magnetic resonance (NMR) spectroscopy, (13)C NMR spectroscopy, and gas chromatography–mass spectrometry (GC–MS). The advantages of the preparation of Schiff bases under microwave irradiation are high yield, shorter reaction time, easy, elimination of side products, and quick product isolation. The synthesized Schiff base derivatives are well known for their biological activity like antibacterial and antifungal activity.
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spelling pubmed-98355182023-01-13 Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst Manjare, Satish B. Mahadik, Rakesh K. Manval, Kalpesh S. More, Prajal P. Dalvi, Siddhesh S. ACS Omega [Image: see text] The Schiff bases were prepared with aromatic aldehyde and aromatic amine using cashew shell extract as a catalyst under microwave irradiation. This reaction is rapid, efficient, and solvent-free and involves the one-pot synthesis of Schiff bases under microwave irradiation. The synthesized Schiff bases were characterized by Fourier transform infrared (FTIR) spectroscopy, (1)H nuclear magnetic resonance (NMR) spectroscopy, (13)C NMR spectroscopy, and gas chromatography–mass spectrometry (GC–MS). The advantages of the preparation of Schiff bases under microwave irradiation are high yield, shorter reaction time, easy, elimination of side products, and quick product isolation. The synthesized Schiff base derivatives are well known for their biological activity like antibacterial and antifungal activity. American Chemical Society 2022-12-20 /pmc/articles/PMC9835518/ /pubmed/36643449 http://dx.doi.org/10.1021/acsomega.2c05187 Text en © 2022 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by-nc-nd/4.0/Permits non-commercial access and re-use, provided that author attribution and integrity are maintained; but does not permit creation of adaptations or other derivative works (https://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Manjare, Satish B.
Mahadik, Rakesh K.
Manval, Kalpesh S.
More, Prajal P.
Dalvi, Siddhesh S.
Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst
title Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst
title_full Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst
title_fullStr Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst
title_full_unstemmed Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst
title_short Microwave-Assisted Rapid and Green Synthesis of Schiff Bases Using Cashew Shell Extract as a Natural Acid Catalyst
title_sort microwave-assisted rapid and green synthesis of schiff bases using cashew shell extract as a natural acid catalyst
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9835518/
https://www.ncbi.nlm.nih.gov/pubmed/36643449
http://dx.doi.org/10.1021/acsomega.2c05187
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