Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film

Hydrogen-bonded organic frameworks (HOFs) are assembled via non-covalent secondary interactions that are scintillating examples of porous crystalline materials. This protocol highlights the synthesis and characterization of U selective, permanently porous, hydrolytically stable single-component (CSM...

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Autores principales: Marvaniya, Karan, Maurya, Ashish, Dobariya, Priyanka, Patel, Ketan, Kushwaha, Shilpi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Protocol
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9843254/
https://www.ncbi.nlm.nih.gov/pubmed/36633954
http://dx.doi.org/10.1016/j.xpro.2022.102006
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author Marvaniya, Karan
Maurya, Ashish
Dobariya, Priyanka
Patel, Ketan
Kushwaha, Shilpi
author_facet Marvaniya, Karan
Maurya, Ashish
Dobariya, Priyanka
Patel, Ketan
Kushwaha, Shilpi
author_sort Marvaniya, Karan
collection PubMed
description Hydrogen-bonded organic frameworks (HOFs) are assembled via non-covalent secondary interactions that are scintillating examples of porous crystalline materials. This protocol highlights the synthesis and characterization of U selective, permanently porous, hydrolytically stable single-component (CSMCRI)HOF-1. We describe the steps to synthesize hydrogen bonding motif and single crystals of (CSMCRI)HOF-1. We then detail the preparation of large-area free-standing thin film of (CSMCRI)HOF-1 (TFCH). Finally, we describe the assessment of the hydrolytic stability of (CSMCRI)HOF-1 and TFCH. For complete details on the use and execution of this protocol, please refer to Kaushik et al. (2022).(1)
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spelling pubmed-98432542023-01-18 Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film Marvaniya, Karan Maurya, Ashish Dobariya, Priyanka Patel, Ketan Kushwaha, Shilpi STAR Protoc Protocol Hydrogen-bonded organic frameworks (HOFs) are assembled via non-covalent secondary interactions that are scintillating examples of porous crystalline materials. This protocol highlights the synthesis and characterization of U selective, permanently porous, hydrolytically stable single-component (CSMCRI)HOF-1. We describe the steps to synthesize hydrogen bonding motif and single crystals of (CSMCRI)HOF-1. We then detail the preparation of large-area free-standing thin film of (CSMCRI)HOF-1 (TFCH). Finally, we describe the assessment of the hydrolytic stability of (CSMCRI)HOF-1 and TFCH. For complete details on the use and execution of this protocol, please refer to Kaushik et al. (2022).(1) Elsevier 2023-01-11 /pmc/articles/PMC9843254/ /pubmed/36633954 http://dx.doi.org/10.1016/j.xpro.2022.102006 Text en © 2022 The Authors https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Protocol
Marvaniya, Karan
Maurya, Ashish
Dobariya, Priyanka
Patel, Ketan
Kushwaha, Shilpi
Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
title Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
title_full Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
title_fullStr Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
title_full_unstemmed Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
title_short Protocol for the synthesis and use of U selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
title_sort protocol for the synthesis and use of u selective hydrogen-bonded organic framework to prepare large-area free-standing thin film
topic Protocol
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9843254/
https://www.ncbi.nlm.nih.gov/pubmed/36633954
http://dx.doi.org/10.1016/j.xpro.2022.102006
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