Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization

In this communication, we describe the first analytical method for the determination of free histidine in hair care products (shampoos and conditioners). Cation-exchange chromatography combined with postcolumn derivatization and fluorimetric detection enabled the accurate (recovery: 83.5–114.8%) and...

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Autores principales: Tsiasioti, Apostolia, Zacharis, Constantinos K., Tzanavaras, Paraskevas D.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Communication
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9863815/
https://www.ncbi.nlm.nih.gov/pubmed/36677945
http://dx.doi.org/10.3390/molecules28020888
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author Tsiasioti, Apostolia
Zacharis, Constantinos K.
Tzanavaras, Paraskevas D.
author_facet Tsiasioti, Apostolia
Zacharis, Constantinos K.
Tzanavaras, Paraskevas D.
author_sort Tsiasioti, Apostolia
collection PubMed
description In this communication, we describe the first analytical method for the determination of free histidine in hair care products (shampoos and conditioners). Cation-exchange chromatography combined with postcolumn derivatization and fluorimetric detection enabled the accurate (recovery: 83.5–114.8%) and precise (2.4–5.6% RSD) determination of free histidine without matrix interferences at concentration levels down to 1.5 mg kg(−1). Real commercially available samples were found to contain the amino acid at levels ranging between 70 and 535 mg kg(−1).
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spelling pubmed-98638152023-01-22 Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization Tsiasioti, Apostolia Zacharis, Constantinos K. Tzanavaras, Paraskevas D. Molecules Communication In this communication, we describe the first analytical method for the determination of free histidine in hair care products (shampoos and conditioners). Cation-exchange chromatography combined with postcolumn derivatization and fluorimetric detection enabled the accurate (recovery: 83.5–114.8%) and precise (2.4–5.6% RSD) determination of free histidine without matrix interferences at concentration levels down to 1.5 mg kg(−1). Real commercially available samples were found to contain the amino acid at levels ranging between 70 and 535 mg kg(−1). MDPI 2023-01-16 /pmc/articles/PMC9863815/ /pubmed/36677945 http://dx.doi.org/10.3390/molecules28020888 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Communication
Tsiasioti, Apostolia
Zacharis, Constantinos K.
Tzanavaras, Paraskevas D.
Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization
title Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization
title_full Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization
title_fullStr Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization
title_full_unstemmed Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization
title_short Determination of Free Histidine in Complex Hair Care Products with Minimum Sample Preparation Using Cation-Exchange Chromatography and Post Column Derivatization
title_sort determination of free histidine in complex hair care products with minimum sample preparation using cation-exchange chromatography and post column derivatization
topic Communication
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9863815/
https://www.ncbi.nlm.nih.gov/pubmed/36677945
http://dx.doi.org/10.3390/molecules28020888
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