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Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System

Curing processes for carbon-fiber-reinforced polymer composites via microwave heating are promising alternatives to conventional thermal curing because this technology results in nonhomogeneous temperature distributions, which hinder its further development in industries. This paper proposes a novel...

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Autores principales: Chen, Kaihua, Zhao, Guozhen, Chen, Jing, Zhu, Xiaobao, Guo, Shenghui
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9864177/
https://www.ncbi.nlm.nih.gov/pubmed/36676442
http://dx.doi.org/10.3390/ma16020705
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author Chen, Kaihua
Zhao, Guozhen
Chen, Jing
Zhu, Xiaobao
Guo, Shenghui
author_facet Chen, Kaihua
Zhao, Guozhen
Chen, Jing
Zhu, Xiaobao
Guo, Shenghui
author_sort Chen, Kaihua
collection PubMed
description Curing processes for carbon-fiber-reinforced polymer composites via microwave heating are promising alternatives to conventional thermal curing because this technology results in nonhomogeneous temperature distributions, which hinder its further development in industries. This paper proposes a novel method for improving heating homogeneities by employing three-dimensional motion with respect to the prepreg laminate used in the microwave field by using a recently developed microwave system. The maximum temperature deviation on the surface of the laminate can be controlled within 8.7 °C during the entire curing process, and it produces an average heating rate of 1.42 °C/min. The FT−IR analyses indicate that microwave heating would slightly influence hydroxyl and methylene contents in the cured laminate. The DMA measurements demonstrate that the glass transition temperatures can be improved by applying proper microwave-curing processes. Optical microscopy and mechanical tests reveal that curing the prepreg laminate by using a multistep curing process that initially cures the laminate at the resin’s lowest viscosity for 10 min followed by curing the laminate at a high temperature for a short period of time would be favorable for yielding a sample with low void contents and the desired mechanical properties. All these analyses are supposed to prove the feasibility of controlling the temperature difference during microwave-curing processes within a reasonable range and provide a cured laminate with improved properties compared with conventional thermally cured products.
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spelling pubmed-98641772023-01-22 Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System Chen, Kaihua Zhao, Guozhen Chen, Jing Zhu, Xiaobao Guo, Shenghui Materials (Basel) Article Curing processes for carbon-fiber-reinforced polymer composites via microwave heating are promising alternatives to conventional thermal curing because this technology results in nonhomogeneous temperature distributions, which hinder its further development in industries. This paper proposes a novel method for improving heating homogeneities by employing three-dimensional motion with respect to the prepreg laminate used in the microwave field by using a recently developed microwave system. The maximum temperature deviation on the surface of the laminate can be controlled within 8.7 °C during the entire curing process, and it produces an average heating rate of 1.42 °C/min. The FT−IR analyses indicate that microwave heating would slightly influence hydroxyl and methylene contents in the cured laminate. The DMA measurements demonstrate that the glass transition temperatures can be improved by applying proper microwave-curing processes. Optical microscopy and mechanical tests reveal that curing the prepreg laminate by using a multistep curing process that initially cures the laminate at the resin’s lowest viscosity for 10 min followed by curing the laminate at a high temperature for a short period of time would be favorable for yielding a sample with low void contents and the desired mechanical properties. All these analyses are supposed to prove the feasibility of controlling the temperature difference during microwave-curing processes within a reasonable range and provide a cured laminate with improved properties compared with conventional thermally cured products. MDPI 2023-01-11 /pmc/articles/PMC9864177/ /pubmed/36676442 http://dx.doi.org/10.3390/ma16020705 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Chen, Kaihua
Zhao, Guozhen
Chen, Jing
Zhu, Xiaobao
Guo, Shenghui
Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System
title Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System
title_full Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System
title_fullStr Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System
title_full_unstemmed Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System
title_short Improvements in Temperature Uniformity in Carbon Fiber Composites during Microwave-Curing Processes via a Recently Developed Microwave Equipped with a Three-Dimensional Motion System
title_sort improvements in temperature uniformity in carbon fiber composites during microwave-curing processes via a recently developed microwave equipped with a three-dimensional motion system
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9864177/
https://www.ncbi.nlm.nih.gov/pubmed/36676442
http://dx.doi.org/10.3390/ma16020705
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