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Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression
The hot compression experiment of homogenized Al−5.2Mg−0.6Mn−0.29Zn−0.16Er–0.12Zr alloy was carried out by the Gleeble-3500 thermal simulation testing system. The deformation behavior in temperatures of 350~500 ℃ and deformation rates of 0.01~10 s(−1) was studied. The relationship between stress and...
Autores principales: | , , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9866373/ https://www.ncbi.nlm.nih.gov/pubmed/36676594 http://dx.doi.org/10.3390/ma16020858 |
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author | Wu, Minbao Wei, Wu Zuo, Rui Wen, Shengping Shi, Wei Zhou, Xiaorong Wu, Xiaolan Gao, Kunyuan Huang, Hui Nie, Zuoren |
author_facet | Wu, Minbao Wei, Wu Zuo, Rui Wen, Shengping Shi, Wei Zhou, Xiaorong Wu, Xiaolan Gao, Kunyuan Huang, Hui Nie, Zuoren |
author_sort | Wu, Minbao |
collection | PubMed |
description | The hot compression experiment of homogenized Al−5.2Mg−0.6Mn−0.29Zn−0.16Er–0.12Zr alloy was carried out by the Gleeble-3500 thermal simulation testing system. The deformation behavior in temperatures of 350~500 ℃ and deformation rates of 0.01~10 s(−1) was studied. The relationship between stress and strain rate and deformation temperature was analyzed. The constitutive equation of alloy high-temperature deformation was constructed by the Zener–Hollomon method, and the hot working diagram with the true strain of 0.2 and 0.5 was constructed according to the dynamic material model. The research results show that flow stress has a positive correlation with strain rate and a negative correlation with temperature. The steady flow stress during deformation can be described by a hyperbolic sinusoidal constitutive equation. Adding Er and Zr into Al−Mg alloy can not only refine grains and strengthen precipitation but also form a core–shell Al(3)(Er, Zr) phase. In the deformation process, Al(3)(Er, Zr) precipitates can pin dislocations and inhibit dynamic recrystallization (DRX). Dynamic recovery (DRV) is dominant during hot deformation. The mechanism of dynamic recovery is dislocation motion. At high temperatures, Al(3)(Er, Zr) can also inhibit grain coarsening. The average hot deformation activation energy of the alloy is 203.7 kJ/mol. This high activation energy can be due to the pinning effect of Er and Zr precipitates. The processing map of the alloy was analyzed and combined with the observation of microstructure, the hot deformation instability zone of the alloy was determined, and the suitable process parameters for hot deformation were obtained, which were 450~480 °C, and the strain rate is 0.01~0.09 s(−1). |
format | Online Article Text |
id | pubmed-9866373 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-98663732023-01-22 Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression Wu, Minbao Wei, Wu Zuo, Rui Wen, Shengping Shi, Wei Zhou, Xiaorong Wu, Xiaolan Gao, Kunyuan Huang, Hui Nie, Zuoren Materials (Basel) Article The hot compression experiment of homogenized Al−5.2Mg−0.6Mn−0.29Zn−0.16Er–0.12Zr alloy was carried out by the Gleeble-3500 thermal simulation testing system. The deformation behavior in temperatures of 350~500 ℃ and deformation rates of 0.01~10 s(−1) was studied. The relationship between stress and strain rate and deformation temperature was analyzed. The constitutive equation of alloy high-temperature deformation was constructed by the Zener–Hollomon method, and the hot working diagram with the true strain of 0.2 and 0.5 was constructed according to the dynamic material model. The research results show that flow stress has a positive correlation with strain rate and a negative correlation with temperature. The steady flow stress during deformation can be described by a hyperbolic sinusoidal constitutive equation. Adding Er and Zr into Al−Mg alloy can not only refine grains and strengthen precipitation but also form a core–shell Al(3)(Er, Zr) phase. In the deformation process, Al(3)(Er, Zr) precipitates can pin dislocations and inhibit dynamic recrystallization (DRX). Dynamic recovery (DRV) is dominant during hot deformation. The mechanism of dynamic recovery is dislocation motion. At high temperatures, Al(3)(Er, Zr) can also inhibit grain coarsening. The average hot deformation activation energy of the alloy is 203.7 kJ/mol. This high activation energy can be due to the pinning effect of Er and Zr precipitates. The processing map of the alloy was analyzed and combined with the observation of microstructure, the hot deformation instability zone of the alloy was determined, and the suitable process parameters for hot deformation were obtained, which were 450~480 °C, and the strain rate is 0.01~0.09 s(−1). MDPI 2023-01-16 /pmc/articles/PMC9866373/ /pubmed/36676594 http://dx.doi.org/10.3390/ma16020858 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Wu, Minbao Wei, Wu Zuo, Rui Wen, Shengping Shi, Wei Zhou, Xiaorong Wu, Xiaolan Gao, Kunyuan Huang, Hui Nie, Zuoren Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression |
title | Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression |
title_full | Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression |
title_fullStr | Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression |
title_full_unstemmed | Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression |
title_short | Effect of Zr and Er Addition on the Microstructural Evolution of a Novel Al−Mg−Zn−Er−Zr Alloy during Hot Compression |
title_sort | effect of zr and er addition on the microstructural evolution of a novel al−mg−zn−er−zr alloy during hot compression |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9866373/ https://www.ncbi.nlm.nih.gov/pubmed/36676594 http://dx.doi.org/10.3390/ma16020858 |
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