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Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor

The Spatz neutron beam instrument is the second time-of-flight neutron reflectometer to be installed at the OPAL research reactor. The instrument was formerly the V18 BioRef reflectometer at the BER-II reactor in Berlin and was transferred to Australia in 2016. Subsequently the instrument was re-ins...

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Detalles Bibliográficos
Autores principales: Le Brun, Anton P., Huang, Tzu-Yen, Pullen, Stewart, Nelson, Andrew R. J., Spedding, James, Holt, Stephen A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9901927/
https://www.ncbi.nlm.nih.gov/pubmed/36777140
http://dx.doi.org/10.1107/S160057672201086X
Descripción
Sumario:The Spatz neutron beam instrument is the second time-of-flight neutron reflectometer to be installed at the OPAL research reactor. The instrument was formerly the V18 BioRef reflectometer at the BER-II reactor in Berlin and was transferred to Australia in 2016. Subsequently the instrument was re-installed in the neutron guide hall of the OPAL reactor at the end position of the CG2B cold-neutron guide and recommissioned. The instrument performance has not been compromised by the move, with reflectivity achieved down to 10(−7) and good counting statistics within a reasonable time frame using a wavelength range of 2–20 Å. Several different samples at the solid–air interface and the solid–liquid interface have been measured to demonstrate the instrument’s capabilities.