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Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor
The Spatz neutron beam instrument is the second time-of-flight neutron reflectometer to be installed at the OPAL research reactor. The instrument was formerly the V18 BioRef reflectometer at the BER-II reactor in Berlin and was transferred to Australia in 2016. Subsequently the instrument was re-ins...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9901927/ https://www.ncbi.nlm.nih.gov/pubmed/36777140 http://dx.doi.org/10.1107/S160057672201086X |
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author | Le Brun, Anton P. Huang, Tzu-Yen Pullen, Stewart Nelson, Andrew R. J. Spedding, James Holt, Stephen A. |
author_facet | Le Brun, Anton P. Huang, Tzu-Yen Pullen, Stewart Nelson, Andrew R. J. Spedding, James Holt, Stephen A. |
author_sort | Le Brun, Anton P. |
collection | PubMed |
description | The Spatz neutron beam instrument is the second time-of-flight neutron reflectometer to be installed at the OPAL research reactor. The instrument was formerly the V18 BioRef reflectometer at the BER-II reactor in Berlin and was transferred to Australia in 2016. Subsequently the instrument was re-installed in the neutron guide hall of the OPAL reactor at the end position of the CG2B cold-neutron guide and recommissioned. The instrument performance has not been compromised by the move, with reflectivity achieved down to 10(−7) and good counting statistics within a reasonable time frame using a wavelength range of 2–20 Å. Several different samples at the solid–air interface and the solid–liquid interface have been measured to demonstrate the instrument’s capabilities. |
format | Online Article Text |
id | pubmed-9901927 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-99019272023-02-10 Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor Le Brun, Anton P. Huang, Tzu-Yen Pullen, Stewart Nelson, Andrew R. J. Spedding, James Holt, Stephen A. J Appl Crystallogr Research Papers The Spatz neutron beam instrument is the second time-of-flight neutron reflectometer to be installed at the OPAL research reactor. The instrument was formerly the V18 BioRef reflectometer at the BER-II reactor in Berlin and was transferred to Australia in 2016. Subsequently the instrument was re-installed in the neutron guide hall of the OPAL reactor at the end position of the CG2B cold-neutron guide and recommissioned. The instrument performance has not been compromised by the move, with reflectivity achieved down to 10(−7) and good counting statistics within a reasonable time frame using a wavelength range of 2–20 Å. Several different samples at the solid–air interface and the solid–liquid interface have been measured to demonstrate the instrument’s capabilities. International Union of Crystallography 2023-02-01 /pmc/articles/PMC9901927/ /pubmed/36777140 http://dx.doi.org/10.1107/S160057672201086X Text en © Anton Le Brun et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Le Brun, Anton P. Huang, Tzu-Yen Pullen, Stewart Nelson, Andrew R. J. Spedding, James Holt, Stephen A. Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor |
title | Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor |
title_full | Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor |
title_fullStr | Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor |
title_full_unstemmed | Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor |
title_short | Spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the OPAL research reactor |
title_sort | spatz: the time-of-flight neutron reflectometer with vertical sample geometry at the opal research reactor |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9901927/ https://www.ncbi.nlm.nih.gov/pubmed/36777140 http://dx.doi.org/10.1107/S160057672201086X |
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