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Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants

Magnesium hydroxide (MOH) is a widely used inorganic chemical owing to its various properties. Hence, researchers have long studied its synthesis and its unique features. However, the morphological consequences have rarely been studied. Despite having several benefits for synthesizing nanoparticles,...

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Autores principales: Rajabimashhadi, Zahra, Naghizadeh, Rahim, Zolriasatein, Ashkan, Esposito Corcione, Carola
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9919068/
https://www.ncbi.nlm.nih.gov/pubmed/36770415
http://dx.doi.org/10.3390/nano13030454
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author Rajabimashhadi, Zahra
Naghizadeh, Rahim
Zolriasatein, Ashkan
Esposito Corcione, Carola
author_facet Rajabimashhadi, Zahra
Naghizadeh, Rahim
Zolriasatein, Ashkan
Esposito Corcione, Carola
author_sort Rajabimashhadi, Zahra
collection PubMed
description Magnesium hydroxide (MOH) is a widely used inorganic chemical owing to its various properties. Hence, researchers have long studied its synthesis and its unique features. However, the morphological consequences have rarely been studied. Despite having several benefits for synthesizing nanoparticles, the hydrothermal method’s main drawbacks are its lengthy processing time and the high cost of raw materials. This research aimed to use more easily obtainable raw materials in a reasonably short time to synthesize MOH in various morphologies. For this purpose, we prepared different samples using the same hydrothermal method to investigate the effects of the precursor and surfactant on the structure, morphology, and size of MOH particles. The results of XRD and FTIR analysis demonstrated that a temperature of 180 °C and a duration of 18 h is not sufficient for MgO as a precursor to obtaining MOH in the hydrothermal method. However, in the presence of different surfactants, MgCl [Formula: see text] resulted in nanoparticles with hexagonal structure and plate, flake, spherical, and disc morphologies.
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spelling pubmed-99190682023-02-12 Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants Rajabimashhadi, Zahra Naghizadeh, Rahim Zolriasatein, Ashkan Esposito Corcione, Carola Nanomaterials (Basel) Article Magnesium hydroxide (MOH) is a widely used inorganic chemical owing to its various properties. Hence, researchers have long studied its synthesis and its unique features. However, the morphological consequences have rarely been studied. Despite having several benefits for synthesizing nanoparticles, the hydrothermal method’s main drawbacks are its lengthy processing time and the high cost of raw materials. This research aimed to use more easily obtainable raw materials in a reasonably short time to synthesize MOH in various morphologies. For this purpose, we prepared different samples using the same hydrothermal method to investigate the effects of the precursor and surfactant on the structure, morphology, and size of MOH particles. The results of XRD and FTIR analysis demonstrated that a temperature of 180 °C and a duration of 18 h is not sufficient for MgO as a precursor to obtaining MOH in the hydrothermal method. However, in the presence of different surfactants, MgCl [Formula: see text] resulted in nanoparticles with hexagonal structure and plate, flake, spherical, and disc morphologies. MDPI 2023-01-22 /pmc/articles/PMC9919068/ /pubmed/36770415 http://dx.doi.org/10.3390/nano13030454 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Rajabimashhadi, Zahra
Naghizadeh, Rahim
Zolriasatein, Ashkan
Esposito Corcione, Carola
Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants
title Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants
title_full Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants
title_fullStr Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants
title_full_unstemmed Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants
title_short Novel Synthesis of Nano Mg(OH)(2) by Means of Hydrothermal Method with Different Surfactants
title_sort novel synthesis of nano mg(oh)(2) by means of hydrothermal method with different surfactants
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9919068/
https://www.ncbi.nlm.nih.gov/pubmed/36770415
http://dx.doi.org/10.3390/nano13030454
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