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Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion

Laser powder bed fusion (L-PBF) has attracted great interest in recent years due to its ability to produce intricate parts beyond the capabilities of traditional manufacturing processes. L-PBF processed biomedical implants are usually made of commercial pure titanium (CP-Ti) or its alloys. However,...

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Autores principales: Wu, Po-Kuan, Lin, Wei-Ting, Lin, Jia-Wei, Tran, Hong-Chuong, Kuo, Tsung-Yuan, Chien, Chi-Sheng, Vo, Vi-Long, Lin, Ru-Li
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9964098/
https://www.ncbi.nlm.nih.gov/pubmed/36837132
http://dx.doi.org/10.3390/ma16041502
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author Wu, Po-Kuan
Lin, Wei-Ting
Lin, Jia-Wei
Tran, Hong-Chuong
Kuo, Tsung-Yuan
Chien, Chi-Sheng
Vo, Vi-Long
Lin, Ru-Li
author_facet Wu, Po-Kuan
Lin, Wei-Ting
Lin, Jia-Wei
Tran, Hong-Chuong
Kuo, Tsung-Yuan
Chien, Chi-Sheng
Vo, Vi-Long
Lin, Ru-Li
author_sort Wu, Po-Kuan
collection PubMed
description Laser powder bed fusion (L-PBF) has attracted great interest in recent years due to its ability to produce intricate parts beyond the capabilities of traditional manufacturing processes. L-PBF processed biomedical implants are usually made of commercial pure titanium (CP-Ti) or its alloys. However, both alloys are naturally bio-inert, and thus reduce the formation of apatite as implants are put into the human body. Accordingly, in an attempt to improve the bioactivity of the materials used for making orthopedic implants, the present study decomposed fluorapatite material (FA, (Ca(10)(PO(4))(6)F(2))) into the form of nano-powder and mixed this powder with CP-Ti powder in two different ratios (99%Ti + 1%FA (Ti-1%FA) and 98%Ti + 2%FA (Ti-2%FA)) to form powder material for the L-PBF process. Experimental trials were conducted to establish the optimal processing conditions (i.e., laser power, scanning speed and hatching space) of the L-PBF process for the two powder mixtures and the original CP-Ti powder with no FA addition. The optimal parameters were then used to produce tensile test specimens in order to evaluate the mechanical properties of the different samples. The hardness of the various samples was also examined by micro-Vickers hardness tests. The tensile strength of the Ti-1%FA sample (850 MPa) was found to be far higher than that of the CP-Ti sample (513 MPa). Furthermore, the yield strength of the Ti-1%FA sample (785 MPa) was also much higher than that of the CP-Ti sample (472 MPa). However, the elongation of the Ti-1%FA sample (6.27 %) was significantly lower than that of the CP-Ti sample (16.17%). Finally, the hardness values of the Ti-1%FA and Ti-2%FA samples were around 63.8% and 109.4%, respectively, higher than that of the CP-Ti sample.
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spelling pubmed-99640982023-02-26 Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion Wu, Po-Kuan Lin, Wei-Ting Lin, Jia-Wei Tran, Hong-Chuong Kuo, Tsung-Yuan Chien, Chi-Sheng Vo, Vi-Long Lin, Ru-Li Materials (Basel) Article Laser powder bed fusion (L-PBF) has attracted great interest in recent years due to its ability to produce intricate parts beyond the capabilities of traditional manufacturing processes. L-PBF processed biomedical implants are usually made of commercial pure titanium (CP-Ti) or its alloys. However, both alloys are naturally bio-inert, and thus reduce the formation of apatite as implants are put into the human body. Accordingly, in an attempt to improve the bioactivity of the materials used for making orthopedic implants, the present study decomposed fluorapatite material (FA, (Ca(10)(PO(4))(6)F(2))) into the form of nano-powder and mixed this powder with CP-Ti powder in two different ratios (99%Ti + 1%FA (Ti-1%FA) and 98%Ti + 2%FA (Ti-2%FA)) to form powder material for the L-PBF process. Experimental trials were conducted to establish the optimal processing conditions (i.e., laser power, scanning speed and hatching space) of the L-PBF process for the two powder mixtures and the original CP-Ti powder with no FA addition. The optimal parameters were then used to produce tensile test specimens in order to evaluate the mechanical properties of the different samples. The hardness of the various samples was also examined by micro-Vickers hardness tests. The tensile strength of the Ti-1%FA sample (850 MPa) was found to be far higher than that of the CP-Ti sample (513 MPa). Furthermore, the yield strength of the Ti-1%FA sample (785 MPa) was also much higher than that of the CP-Ti sample (472 MPa). However, the elongation of the Ti-1%FA sample (6.27 %) was significantly lower than that of the CP-Ti sample (16.17%). Finally, the hardness values of the Ti-1%FA and Ti-2%FA samples were around 63.8% and 109.4%, respectively, higher than that of the CP-Ti sample. MDPI 2023-02-10 /pmc/articles/PMC9964098/ /pubmed/36837132 http://dx.doi.org/10.3390/ma16041502 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Wu, Po-Kuan
Lin, Wei-Ting
Lin, Jia-Wei
Tran, Hong-Chuong
Kuo, Tsung-Yuan
Chien, Chi-Sheng
Vo, Vi-Long
Lin, Ru-Li
Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion
title Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion
title_full Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion
title_fullStr Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion
title_full_unstemmed Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion
title_short Mechanical Properties of Titanium/Nano-Fluorapatite Parts Produced by Laser Powder Bed Fusion
title_sort mechanical properties of titanium/nano-fluorapatite parts produced by laser powder bed fusion
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9964098/
https://www.ncbi.nlm.nih.gov/pubmed/36837132
http://dx.doi.org/10.3390/ma16041502
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