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A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy

Recently, there has been growing interest in using lightwave-driven scanning probe microscopy (LD-SPM) to break through the Abbe diffraction limit of focusing, yielding insight into various energy couplings and conversion processes and revealing the internal information of matter. We describe a comp...

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Autores principales: Xiang, Kui, Xie, Caihong, Feng, Qiyuan, Wang, Ze, Dai, Guangbin, Wang, Jihao, Zhang, Jing, Meng, Wenjie, Hou, Yubin, Lu, Qingyou, Lu, Yalin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9964935/
https://www.ncbi.nlm.nih.gov/pubmed/36838078
http://dx.doi.org/10.3390/mi14020378
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author Xiang, Kui
Xie, Caihong
Feng, Qiyuan
Wang, Ze
Dai, Guangbin
Wang, Jihao
Zhang, Jing
Meng, Wenjie
Hou, Yubin
Lu, Qingyou
Lu, Yalin
author_facet Xiang, Kui
Xie, Caihong
Feng, Qiyuan
Wang, Ze
Dai, Guangbin
Wang, Jihao
Zhang, Jing
Meng, Wenjie
Hou, Yubin
Lu, Qingyou
Lu, Yalin
author_sort Xiang, Kui
collection PubMed
description Recently, there has been growing interest in using lightwave-driven scanning probe microscopy (LD-SPM) to break through the Abbe diffraction limit of focusing, yielding insight into various energy couplings and conversion processes and revealing the internal information of matter. We describe a compact and efficient optical cryostat designed for LD-SPM testing under magnetic fields. The exceptional multilayer radiation shielding insert (MRSI) forms an excellent temperature gradient when filled with heat conducting gas, which removes the requirement to install an optical window in the liquid helium cooling shell. This not only critically avoids the vibration and thermal drift caused by solid heat conduction but also minimizes light transmission loss. The application of gate valves and bellows allows a simpler and more effective replacement of the sample and working cell in the test cavity. ANSYS software is used for steady-state thermal analysis of the MRSI to obtain the temperature distribution and heat transfer rate, and the necessity of the flexible copper shielding strips is illustrated by the simulations. The topography and magnetic domain images of 45 nm-thick La(0.67)Ca(0.33)MnO(3) thin films on NdGaO(3)(001) substrates under a magnetic field were obtained by a self-made lightwave-driven magnetic force microscope in this cryostat. The resolution and noise spectra during imaging reveal temperature stability and low vibration throughout the cryostat. The experience acquired during the development of this cryostat will help to establish cryostats of similar types for a variety of optic applications requiring the use of cryogenic temperatures.
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spelling pubmed-99649352023-02-26 A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy Xiang, Kui Xie, Caihong Feng, Qiyuan Wang, Ze Dai, Guangbin Wang, Jihao Zhang, Jing Meng, Wenjie Hou, Yubin Lu, Qingyou Lu, Yalin Micromachines (Basel) Article Recently, there has been growing interest in using lightwave-driven scanning probe microscopy (LD-SPM) to break through the Abbe diffraction limit of focusing, yielding insight into various energy couplings and conversion processes and revealing the internal information of matter. We describe a compact and efficient optical cryostat designed for LD-SPM testing under magnetic fields. The exceptional multilayer radiation shielding insert (MRSI) forms an excellent temperature gradient when filled with heat conducting gas, which removes the requirement to install an optical window in the liquid helium cooling shell. This not only critically avoids the vibration and thermal drift caused by solid heat conduction but also minimizes light transmission loss. The application of gate valves and bellows allows a simpler and more effective replacement of the sample and working cell in the test cavity. ANSYS software is used for steady-state thermal analysis of the MRSI to obtain the temperature distribution and heat transfer rate, and the necessity of the flexible copper shielding strips is illustrated by the simulations. The topography and magnetic domain images of 45 nm-thick La(0.67)Ca(0.33)MnO(3) thin films on NdGaO(3)(001) substrates under a magnetic field were obtained by a self-made lightwave-driven magnetic force microscope in this cryostat. The resolution and noise spectra during imaging reveal temperature stability and low vibration throughout the cryostat. The experience acquired during the development of this cryostat will help to establish cryostats of similar types for a variety of optic applications requiring the use of cryogenic temperatures. MDPI 2023-02-02 /pmc/articles/PMC9964935/ /pubmed/36838078 http://dx.doi.org/10.3390/mi14020378 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Xiang, Kui
Xie, Caihong
Feng, Qiyuan
Wang, Ze
Dai, Guangbin
Wang, Jihao
Zhang, Jing
Meng, Wenjie
Hou, Yubin
Lu, Qingyou
Lu, Yalin
A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy
title A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy
title_full A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy
title_fullStr A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy
title_full_unstemmed A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy
title_short A Cryostat Applicable to Long-Wavelength Light-Driven Scanning Probe Microscopy
title_sort cryostat applicable to long-wavelength light-driven scanning probe microscopy
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9964935/
https://www.ncbi.nlm.nih.gov/pubmed/36838078
http://dx.doi.org/10.3390/mi14020378
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