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Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy
Local anodization with a free electrolyte jet is a suitable solution for locally confined surface functionalization without additionally required preparation of the parts. However, the geometrical formation of the anodic oxide layer in jet-based anodization is not yet sufficiently understood. In thi...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9965328/ https://www.ncbi.nlm.nih.gov/pubmed/36837993 http://dx.doi.org/10.3390/mi14020293 |
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author | Quitzke, Susanne Danilov, Igor Martin, André Morgenstern, Roy Lampke, Thomas Schubert, Andreas |
author_facet | Quitzke, Susanne Danilov, Igor Martin, André Morgenstern, Roy Lampke, Thomas Schubert, Andreas |
author_sort | Quitzke, Susanne |
collection | PubMed |
description | Local anodization with a free electrolyte jet is a suitable solution for locally confined surface functionalization without additionally required preparation of the parts. However, the geometrical formation of the anodic oxide layer in jet-based anodization is not yet sufficiently understood. In this study, numerical calculations based on physical descriptions are used to describe the lateral and vertical oxide formation on aluminum alloy EN AW-7075. The required electrical resistance and capacitance were determined by immersion-based anodization and implemented into the numerical simulation model to evaluate the electrical conductivity of the porous layer. The simulation results showed an electrical conductivity of 2.6 × 10(−6) S/m for the porous layer. Subsequently, a model for jet-based anodization was developed and the previous results were implemented to calculate the oxide formation. The simulation results showed decreasing oxide layer thickness at increasing radial distance from the center of the jet, which corresponds to experimental results. The simulation model was validated by varying the current efficiency from 5% to 90%, where similar developments of the anodic oxide layer thickness compared with experimental results were determined at 5%. |
format | Online Article Text |
id | pubmed-9965328 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-99653282023-02-26 Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy Quitzke, Susanne Danilov, Igor Martin, André Morgenstern, Roy Lampke, Thomas Schubert, Andreas Micromachines (Basel) Article Local anodization with a free electrolyte jet is a suitable solution for locally confined surface functionalization without additionally required preparation of the parts. However, the geometrical formation of the anodic oxide layer in jet-based anodization is not yet sufficiently understood. In this study, numerical calculations based on physical descriptions are used to describe the lateral and vertical oxide formation on aluminum alloy EN AW-7075. The required electrical resistance and capacitance were determined by immersion-based anodization and implemented into the numerical simulation model to evaluate the electrical conductivity of the porous layer. The simulation results showed an electrical conductivity of 2.6 × 10(−6) S/m for the porous layer. Subsequently, a model for jet-based anodization was developed and the previous results were implemented to calculate the oxide formation. The simulation results showed decreasing oxide layer thickness at increasing radial distance from the center of the jet, which corresponds to experimental results. The simulation model was validated by varying the current efficiency from 5% to 90%, where similar developments of the anodic oxide layer thickness compared with experimental results were determined at 5%. MDPI 2023-01-22 /pmc/articles/PMC9965328/ /pubmed/36837993 http://dx.doi.org/10.3390/mi14020293 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Quitzke, Susanne Danilov, Igor Martin, André Morgenstern, Roy Lampke, Thomas Schubert, Andreas Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy |
title | Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy |
title_full | Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy |
title_fullStr | Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy |
title_full_unstemmed | Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy |
title_short | Simulation-Assisted Process Design and Experimental Verification of Laterally Confined Oxide Areas Generated with Continuous Electrolytic Free Jet on EN AW-7075 Aluminum Alloy |
title_sort | simulation-assisted process design and experimental verification of laterally confined oxide areas generated with continuous electrolytic free jet on en aw-7075 aluminum alloy |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9965328/ https://www.ncbi.nlm.nih.gov/pubmed/36837993 http://dx.doi.org/10.3390/mi14020293 |
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