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Use of Trifluoro-Acetate Derivatives for GC-MS and GC-MS/MS Quantification of Trace Amounts of Stera-3β,5α,6β-Triols (Tracers of Δ(5)-Sterol Autoxidation) in Environmental Samples

Stera-3β,5α,6β-triols make useful tracers of the autoxidation of Δ(5)-sterols. These compounds are generally analyzed using gas chromatography–mass spectrometry (GC-MS) after silylation. Unfortunately, the 5α hydroxyl groups of these compounds, which are not derivatized by conventional silylation re...

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Detalles Bibliográficos
Autores principales: Aubert, Claude, Rontani, Jean-François
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9967974/
https://www.ncbi.nlm.nih.gov/pubmed/36838534
http://dx.doi.org/10.3390/molecules28041547