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Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design

Mesoporous silica is restricted to organic solvents or other acidic media. The application of mesoporous silica depends on the medium's chemical stability and mechanical properties. It is necessary to stabilize the mesoporous silica material under acidic conditions. The results of the nitrogen...

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Autores principales: Andriayani, Marpongahtun, Muis, Yugia, Pakpahan, Jessica, Daulay, Amru
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9987514/
https://www.ncbi.nlm.nih.gov/pubmed/36891488
http://dx.doi.org/10.1039/d2ra06973c
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author Andriayani,
Marpongahtun,
Muis, Yugia
Pakpahan, Jessica
Daulay, Amru
author_facet Andriayani,
Marpongahtun,
Muis, Yugia
Pakpahan, Jessica
Daulay, Amru
author_sort Andriayani,
collection PubMed
description Mesoporous silica is restricted to organic solvents or other acidic media. The application of mesoporous silica depends on the medium's chemical stability and mechanical properties. It is necessary to stabilize the mesoporous silica material under acidic conditions. The results of the nitrogen adsorption characterization show that MS-50 has a large surface area and porosity, resulting in good mesoporous silica. Using variance analysis (ANOVA) to compare the collected data, the best conditions were found at a pH of 6.32, a Cd(2+) concentration of 25.30 ppm, an adsorbent dose of 0.06 g, and a time of 70.44 min. The Cd(2+) adsorption experiment data best fit the Langmuir isotherm model with the maximum amount of Cd(2+) that MS-50 could absorb being 103.10 mg g(−1).
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spelling pubmed-99875142023-03-07 Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design Andriayani, Marpongahtun, Muis, Yugia Pakpahan, Jessica Daulay, Amru RSC Adv Chemistry Mesoporous silica is restricted to organic solvents or other acidic media. The application of mesoporous silica depends on the medium's chemical stability and mechanical properties. It is necessary to stabilize the mesoporous silica material under acidic conditions. The results of the nitrogen adsorption characterization show that MS-50 has a large surface area and porosity, resulting in good mesoporous silica. Using variance analysis (ANOVA) to compare the collected data, the best conditions were found at a pH of 6.32, a Cd(2+) concentration of 25.30 ppm, an adsorbent dose of 0.06 g, and a time of 70.44 min. The Cd(2+) adsorption experiment data best fit the Langmuir isotherm model with the maximum amount of Cd(2+) that MS-50 could absorb being 103.10 mg g(−1). The Royal Society of Chemistry 2023-03-06 /pmc/articles/PMC9987514/ /pubmed/36891488 http://dx.doi.org/10.1039/d2ra06973c Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/
spellingShingle Chemistry
Andriayani,
Marpongahtun,
Muis, Yugia
Pakpahan, Jessica
Daulay, Amru
Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design
title Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design
title_full Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design
title_fullStr Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design
title_full_unstemmed Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design
title_short Stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of HCl and application of Cd(2+) adsorption optimized by Box–Behnken design
title_sort stability of mesoporous silica using ricinoleic methyl ester as a template with the addition of hcl and application of cd(2+) adsorption optimized by box–behnken design
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9987514/
https://www.ncbi.nlm.nih.gov/pubmed/36891488
http://dx.doi.org/10.1039/d2ra06973c
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