Cargando…

Crystal structures of two 1,2,3,4-tetrahydronaphthalenes obtained during efforts towards the total synthesis of elisabethin A

The two substituted 1,2,3,4-tetrahydronaphthalenes, methyl (R)-3-{(1R,4S)-6-methoxy-4,7-dimethyl-5,8-bis[(triisopropylsilyl)oxy]-1,2,3,4-tetrahydronaphthalen-1-yl}butanoate, C(36)H(66)O(5)Si(2), (2), and methyl (E)-3-{(1R,4S)-8-hydroxy-6-methoxy-4,7-dimethyl-5-[(triisopropylsilyl)...

Descripción completa

Detalles Bibliográficos
Autores principales:	Kaiser, Maximilian, Weil, Matthias, Gärtner, Peter, Enev, Valentin
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	International Union of Crystallography 2023
Materias:	Research Communications
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC9993920/ https://www.ncbi.nlm.nih.gov/pubmed/36909998 http://dx.doi.org/10.1107/S2056989023001226

Ejemplares similares

Efforts toward the Total Synthesis of Elisabethin A
por: Kaiser, Maximilian, et al.
Publicado: (2022)

2-(1,2,3,4-Tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2012)

(E)-2-Cyano-N′-(1,2,3,4-tetrahydronaphthalen-1-ylidene)acetohydrazide
por: Al-Omar, Mohamed A., et al.
Publicado: (2012)

7-Nitro-1,2,3,4-tetrahydronaphthalene-1-spiro-2′-(1,3-dithiane)
por: Fun, Hoong-Kun, et al.
Publicado: (2009)

Crystal structure of 3-benzyl-1-[(1,2,3,4-tetrahydronaphthalen-1-ylidene)amino]thiourea
por: Mohamed, Shaaban K., et al.
Publicado: (2015)

Crystal structure of N-ethyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2017)

2-[(E)-4-Methoxybenzylidene]-1,2,3,4-tetrahydronaphthalen-1-one
por: Asiri, Abdullah M., et al.
Publicado: (2012)

5,6,7,8-Tetrahydronaphthalene-1-carboxylic acid
por: Zou, Pei, et al.
Publicado: (2009)

1-(2,4-Dinitrophenyl)-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazine
por: Danish, M., et al.
Publicado: (2010)

(2E)-2-(Thiophen-2-ylmethylidene)-1,2,3,4-tetrahydronaphthalen-1-one
por: Asiri, Abdullah M., et al.
Publicado: (2012)

Crystal structure of 3-(prop-2-en-1-yl)-1-{[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]amino}thiourea
por: Mague, Joel T., et al.
Publicado: (2015)

(3R,4S)-3,4,8-Trihydroxy-1,2,3,4-tetrahydronaphthalen-1-one monohydrate from Embellisia eureka
por: Ouchbani, Tarik, et al.
Publicado: (2012)

1′,1′′-Dimethyl-4′-(naphthalen-1-yl)-1,2,3,4-tetrahydronaphthalene-2-spiro-3′-pyrrolidine-2′-spiro-3′′-indoline-1,2′′-dione
por: Selvanayagam, S., et al.
Publicado: (2011)

Crystal structure of cis-bis[4-phenyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamidato-κ(2) N (1),S]nickel(II) monohydrate tetrahydrofuran disolvate
por: de Oliveira, Adriano Bof, et al.
Publicado: (2014)

8,8-Diethyl-1,4,5,8-tetrahydronaphthalene-1,4,5-trione
por: Vega, Andrés, et al.
Publicado: (2009)

N-Methyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2014)

N-Phenyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide
por: de Oliveira, Adriano Bof, et al.
Publicado: (2014)

Crystal structure and Hirshfeld surface analysis of (E)-N-[(2-ethoxynaphthalen-1-yl)methylidene]-5,6,7,8-tetrahydronaphthalen-1-amine
por: Kansiz, Sevgi, et al.
Publicado: (2018)

Crystal structure and Hirshfeld surface analysis of (E)-N-[(2-ethoxynaphthalen-1-yl)methylidene]-5,6,7,8-tetrahydronaphthalen-1-amine. Corrigendum
por: Kansiz, Sevgi, et al.
Publicado: (2018)

1,2,3,4-Tetrahydro-1,4-methanonaphthalene-2,3-diol
por: Xu, Jian, et al.
Publicado: (2008)

Crystal structure of (E)-1-(3-benzyl-5-phenyl-1,3-thiazol-2-ylidene)-2-[(E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]hydrazin-1-ium bromide
por: Mohamed, Shaaban K., et al.
Publicado: (2021)

Crystal structure of (E)-2-[(2-bromopyridin-3-yl)methylidene]-6-methoxy-3,4-dihydronaphthalen-1(2H)-one and 3-[(E)-(6-methoxy-1-oxo-1,2,3,4-tetrahydronaphthalen-2-ylidene)methyl]pyridin-2(1H)-one
por: Zingales, Sarah K., et al.
Publicado: (2016)

Crystal structure of 1-tosyl-1,2,3,4-tetrahydroquinoline
por: Jeyaseelan, S., et al.
Publicado: (2014)

Methyl 3,5,5,6,8,8-hexamethyl-5,6,7,8-tetrahydronaphthalene-2-carboxylate (AHTN–COOMe)
por: Kuhlich, Paul, et al.
Publicado: (2011)

Crystal structure of the charge-transfer complex 2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamide–pyrazine-2,3,5,6-tetracarbonitrile (2/1)
por: Beck, Johannes, et al.
Publicado: (2014)

Crystal structure of 1-benzylsulfonyl-1,2,3,4-tetrahydroquinoline
por: Jeyaseelan, S., et al.
Publicado: (2015)

Crystal structure of 1-methanesulfonyl-1,2,3,4-tetrahydroquinoline
por: Jeyaseelan, S., et al.
Publicado: (2015)

Crystal structure of 2-methyl-1,2,3,4-tetrahydroisoquinoline trihydrate
por: Langenohl, Felix, et al.
Publicado: (2020)

1,2,3,4-Tetrahydroisoquinoline-2-sulfonamide
por: Bouasla, Radia, et al.
Publicado: (2008)

(3,5,5,6,8,8-Hexamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)methanol: a possible metabolite of the synthetic musk fragrance AHTN
por: Faust, Rüdiger, et al.
Publicado: (2011)

1′-(4-Bromophenyl)-4′-{4-[(2-oxo-1,2,3,4-tetrahydronaphthalen-2-ylidene)methyl]phenyl}-3′′,4′′-dihydroacenaphthylene-1-spiro-2′-pyrrolidine-3′-spiro-2′′-naphthalene-2,1′′(1H,2′′H)-dione
por: Saravanan, B., et al.
Publicado: (2010)

Methyl 2-((2Z,5Z)-4-oxo-3-phenyl-2-{2-[(1E)-1,2,3,4-tetrahydronaphthalen-1-ylidene]hydrazin-1-ylidene}-1,3-thiazolidin-5-ylidene)acetate
por: Mague, Joel T., et al.
Publicado: (2014)

1,2,3,4-Tetrahydrophenazine 5,10-dioxide
por: Sun, Tao, et al.
Publicado: (2010)

Crystal structure of 3-hydroxymethyl-1,2,3,4-tetrahydroisoquinolin-1-one
por: Caracelli, Ignez, et al.
Publicado: (2015)

Bis(1,2,3,4-tetrahydroquinolin-6-yl)methane
por: Shen, Li, et al.
Publicado: (2008)

A new example of intramolecular C—H⋯Ni anagostic interactions: synthesis, crystal structure and Hirshfeld analysis of cis-bis[4-methyl-2-(1,2,3,4-tetrahydronaphthalen-1-ylidene)hydrazinecarbothioamidato-κ(2) N (1),S]nickel(II) dimethylformamide monosolvate
por: de Oliveira, Adriano Bof, et al.
Publicado: (2017)

2-(1,2,3,4-Tetrahydrophenanthren-1-ylidene)malononitrile
por: Ettenger, George B., et al.
Publicado: (2009)

Crystal structure of 1-[(6-chloropyridin-3-yl)sulfonyl]-1,2,3,4-tetrahydroquinoline
por: Jeyaseelan, S., et al.
Publicado: (2015)

1-(4-Bromo-3,5,5,6,8,8-hexamethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethan-1-one: a precursor for phase-I metabolite of AHTN
por: Kuhlich, Paul, et al.
Publicado: (2013)

Crystal structure of cis-1-(2-methyl-1,2,3,4-tetrahydroquinolin-4-yl)azepan-2-one
por: Pradeep, P. S., et al.
Publicado: (2014)

Cannot write session to /tmp/vufind_sessions/sess_kjeljst27gli8tet87566bvi15