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1521“…ZnO nanoparticles were also obtained when the generated ZnO-starch nanocomposite was calcined at 575 °C. The properties of ZnO-starch nanocomposite and ZnO nanoparticle were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). …”
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1522por Xiang, Tianyu, Xin, Feng, Chen, Jingshuai, Wang, Yuwen, Yin, Xiaohong, Shao, Xiao“…CuO was loaded onto the surface of NaTaO(3) as a cocatalyst by successive impregnation and calcination. The obtained photocatalysts were characterized by XRD, SEM, UV–vis, EDS and XPS and used to photocatalytically reduce CO(2) in isopropanol. …”
Publicado 2016
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1523“…Graphitic-C(3)N(4) nanosheets (CN)/ZnO photocatalysts (CN/ZnO) with different CN loadings were successfully prepared via a simple precipitation-calcination in the presence of exfoliated C(3)N(4) nanosheets. …”
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1524“…Novel three-dimensional hierarchical flower-like TiO(2)/carbon (TiO(2)/C) nanostructures were in-situ synthesized via a solvothermal method involving calcination of organic precursor under inert atmosphere. …”
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1525“…The zinc and cobalt based zeolite imidazole frameworks (BM-ZIFs) encapsulating ultrasmall Pd NPs (2–3 nm) were assembled on PS spheres at room temperature. After calcination at 450 °C, these nanoscale Pd particles were effectively infiltrated on the surface of ZnO/ZnCo(2)O(4) HSs. …”
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1526“…The BNT perovskite phase formed after calcination at 500 °C in air. The deposited thin films were single phase according to X-ray diffraction, and the microstructures of the films shown by electron microscopy were homogeneous and dense. …”
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1527“…The results show that the crystal transformation of alumina is restricted by the doped Cr and facilitated by the doped Fe and Mg, which is transformed from θ-Al(2)O(3) to α-Al(2)O(3) in the calcination process. Meanwhile, the crystal transformation of alumina is strongly restrained by co-doped elements from the chromium-containing alumina sludge. …”
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1528“…Chemical formation of alkoxy groups onto MCM-41 occurs both for calcined and hydroxylated MCM-41 and the alkoxy groups are hydrolytically unstable and can be replaced by silanol groups after exposure to water. …”
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1529por Ren, Hao, Sun, Jiajia, Yu, Ranbo, Yang, Mei, Gu, Lin, Liu, Porun, Zhao, Huijun, Kisailus, David, Wang, Dan“…The TiO(2) nanospheres formed after calcination at 400 °C are composed of ∼7 nm nanoparticles and the shells of the hollow TiO(2) nanospheres are as thin as a single layer of nanoparticles. …”
Publicado 2016
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1530“…The 1D nanowire structure with a high aspect ratio was easily achieved via a magnetic-field-assisted self-assembly of cobalt ion complexes during reduction. After air-calcinations, the Co(3)O(4) nanowires were prepared in large scale and ready to be used as the anode material for lithium-ion batteries. …”
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1531por Zhang, Zhe, Yu, Jiafeng, Zhang, Jixin, Ge, Qingjie, Xu, Hengyong, Dallmann, Felix, Dittmeyer, Roland, Sun, Jian“…This process can ensure the formation of solid solutions as well as avoiding atomic rearrangement during calcination, retaining the lattice oxygen at a metastable and disordered state without vacancies. …”
Publicado 2018
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1532por Xu, Zhenhe, Yu, He, Ai, Feixue, Zhao, Guiyan, Bi, Yanfeng, Huang, Liangliang, Ding, Fu, Sun, Yaguang, Gao, Yu“…In this study, YBO(3): Eu(3+)/Tb(3+) hollow microspheres were fabricated by using a novel multi-step transformation synthetic route for the first time with polystyrene spheres as the template, followed by the combination of a facile homogeneous precipitation method, an ion-exchange process and a calcination process. The results show that the as-obtained YBO(3): Eu(3+)/Tb(3+) hollow spheres have a uniform morphology with an average diameter of 1.65 µm and shell thickness of about 160 nm. …”
Publicado 2018
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1533“…Another two sorts of new membranes SiO(2)/C membrane and hierarchical porous polymer (HPP) membrane, which were obtained by modification of the BPPO-SiO(2) membrane by calcination and etching, were set up in a further study. …”
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1534por Dodoo-Arhin, David, Buabeng, Frederick Paakwah, Mwabora, Julius M., Amaniampong, Prince Nana, Agbe, Henry, Nyankson, Emmanuel, Obada, David Olubiyi, Asiedu, Nana Yaw“…The results show that for catalysts calcined at 300 °C, ∼100 % decomposition of Sudan III dye was observed when Hydrothermal based catalyst was used whiles ∼94 % decomposition of Rhodamine B dye was observed using the sol-gel based catalysts. …”
Publicado 2018
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1535Multifunctional Heterogeneous Catalysts for the Selective Conversion of Glycerol into Methyl Lactate“…The activity of the multifunctional catalytic system was further optimized by tuning the calcination temperature, the gold loading in the Au/CuO catalyst, and the Au/Sn molar ratio, reaching 63% yield of methyl lactate (ML) at 95% glycerol conversion. …”
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1536“…According to X-ray diffraction analysis (XRD), cobalt ferrite was in a single cubic phase after being calcined at 1000 °C for 3 h. Moreover, the lattice constant decreased with increase in aluminum substituents. …”
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1537por Wu, Ming Hao, Li, Kai Lin, Zhang, Xin Yu, Gan, Ping, Ge, Jia Lin, Tian, Dan Ning, Jiang, De Bin, Liu, Xiao Ying, Zhang, Yu Xin“…FeOOH nanosheets on porous diatomite have been successfully prepared by a facile two-step hydrothermal approach for supercapacitors, and then α-Fe(2)O(3) and γ-Fe(2)O(3) nanostructures are obtained via calcination under different atmospheres and temperatures. …”
Publicado 2018
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1538“…Stable bimetallic catalysts composed of CoPt(x)/γ-Al(2)O(3) (x = Pt/Co molar ratio) were synthesized by wet impregnation method followed by calcination and the H(2) reduction. The powders were characterized using XRD, AAS, BET, SEM, EDX, TPR, and TPO techniques. …”
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1539por Xue, Dongping, Wang, Junjun, Wang, Yan, Sun, Guang, Cao, Jianliang, Bala, Hari, Zhang, Zhanying“…Here, WO(3) nanosheets loaded with SnO(2) nanoparticles with a particle size of about 2 nm were prepared by simple impregnation and subsequent calcination using SnO(2) and WO(3)·H(2)O as precursors. …”
Publicado 2019
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1540por Yan, Jianhua, Zhao, Yun, Wang, Xiao, Xia, Shuhui, Zhang, Yuanyuan, Han, Yuhui, Yu, Jianyong, Ding, Bin“…Here, we develop a sol-gel electrospinning technique followed by calcination to create a range of oxide ceramic nanofiber films that exhibit significant softness without fragility after various deformations. …”
Publicado 2019
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