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Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$

We demonstrate the combined use of scanning electron microscopy (SEM) and scanning Hall probe microscopy (SHPM) to analyse inhomogeneities in Nb$_{3}$Sn wires. Inhomogeneities of the A15 phase in Nb$_{3}$Sn sub-elements of a Ti-alloyed Restacked Rod Process wire and a Ta-alloyed Powder-In-Tube wire...

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Detalles Bibliográficos
Autores principales: Pfeiffer, S, Baumgartner, T, Löffler, S, Stöger-Pollach, M, Hopkins, S C, Ballarino, A, Eisterer, M, Bernardi, J
Lenguaje:eng
Publicado: 2023
Materias:
Acceso en línea:https://dx.doi.org/10.1088/1361-6668/acb857
http://cds.cern.ch/record/2853518
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author Pfeiffer, S
Baumgartner, T
Löffler, S
Stöger-Pollach, M
Hopkins, S C
Ballarino, A
Eisterer, M
Bernardi, J
author_facet Pfeiffer, S
Baumgartner, T
Löffler, S
Stöger-Pollach, M
Hopkins, S C
Ballarino, A
Eisterer, M
Bernardi, J
author_sort Pfeiffer, S
collection CERN
description We demonstrate the combined use of scanning electron microscopy (SEM) and scanning Hall probe microscopy (SHPM) to analyse inhomogeneities in Nb$_{3}$Sn wires. Inhomogeneities of the A15 phase in Nb$_{3}$Sn sub-elements of a Ti-alloyed Restacked Rod Process wire and a Ta-alloyed Powder-In-Tube wire are investigated. Microstructural features are examined by SEM, elemental concentration gradients by energy dispersive x-ray spectroscopy (EDX) and the superconducting properties by SHPM. Correlations between the results are analysed to gain information about the impact of inhomogeneities in the microstructure on the superconducting properties. We find considerable differences in geometry and performance between sub-elements, as well as compositional and geometric inhomogeneities of the A15 phase inside single sub-elements. Additionally, simulations of the influence of Sn concentration gradients on the critical current density J $_{c}$ are performed. We also demonstrate the viability of SHPM and EDX for determining the dependence of the critical temperature T $_{c}$ on the Sn concentration and discuss possible performance gains by a reduction of inhomogeneities in Nb$_{3}$Sn wires.
id cern-2853518
institution Organización Europea para la Investigación Nuclear
language eng
publishDate 2023
record_format invenio
spelling cern-28535182023-03-31T12:46:36Zdoi:10.1088/1361-6668/acb857http://cds.cern.ch/record/2853518engPfeiffer, SBaumgartner, TLöffler, SStöger-Pollach, MHopkins, S CBallarino, AEisterer, MBernardi, JAnalysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$Accelerators and Storage RingsWe demonstrate the combined use of scanning electron microscopy (SEM) and scanning Hall probe microscopy (SHPM) to analyse inhomogeneities in Nb$_{3}$Sn wires. Inhomogeneities of the A15 phase in Nb$_{3}$Sn sub-elements of a Ti-alloyed Restacked Rod Process wire and a Ta-alloyed Powder-In-Tube wire are investigated. Microstructural features are examined by SEM, elemental concentration gradients by energy dispersive x-ray spectroscopy (EDX) and the superconducting properties by SHPM. Correlations between the results are analysed to gain information about the impact of inhomogeneities in the microstructure on the superconducting properties. We find considerable differences in geometry and performance between sub-elements, as well as compositional and geometric inhomogeneities of the A15 phase inside single sub-elements. Additionally, simulations of the influence of Sn concentration gradients on the critical current density J $_{c}$ are performed. We also demonstrate the viability of SHPM and EDX for determining the dependence of the critical temperature T $_{c}$ on the Sn concentration and discuss possible performance gains by a reduction of inhomogeneities in Nb$_{3}$Sn wires.Abstract We demonstrate the combined use of scanning electron microscopy (SEM) and scanning Hall probe microscopy (SHPM) to analyse inhomogeneities in Nb3Sn wires. Inhomogeneities of the A15 phase in Nb3Sn sub-elements of a Ti-alloyed Restacked Rod Process wire and a Ta-alloyed Powder-In-Tube wire are investigated. Microstructural features are examined by SEM, elemental concentration gradients by energy dispersive x-ray spectroscopy (EDX) and the superconducting properties by SHPM. Correlations between the results are analysed to gain information about the impact of inhomogeneities in the microstructure on the superconducting properties. We find considerable differences in geometry and performance between sub-elements, as well as compositional and geometric inhomogeneities of the A15 phase inside single sub-elements. Additionally, simulations of the influence of Sn concentration gradients on the critical current density J c are performed. We also demonstrate the viability of SHPM and EDX for determining the dependence of the critical temperature T c on the Sn concentration and discuss possible performance gains by a reduction of inhomogeneities in Nb3Sn wires.oai:cds.cern.ch:28535182023
spellingShingle Accelerators and Storage Rings
Pfeiffer, S
Baumgartner, T
Löffler, S
Stöger-Pollach, M
Hopkins, S C
Ballarino, A
Eisterer, M
Bernardi, J
Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$
title Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$
title_full Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$
title_fullStr Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$
title_full_unstemmed Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$
title_short Analysis of inhomogeneities in Nb$_{3}$Sn wires by combined SEM and SHPM and their impact on J $_{c}$ and T $_{c}$
title_sort analysis of inhomogeneities in nb$_{3}$sn wires by combined sem and shpm and their impact on j $_{c}$ and t $_{c}$
topic Accelerators and Storage Rings
url https://dx.doi.org/10.1088/1361-6668/acb857
http://cds.cern.ch/record/2853518
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