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Residual proton line width under refocused frequency-switched Lee-Goldburg decoupling in MAS NMR

Despite many decades of research, homonuclear decoupling in solid-state NMR under magic-angle spinning (MAS) has yet to reach a point where the achievable proton line widths become comparable to the resolution obtained in solution-state NMR. This makes the precise determination of isotropic chemical...

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Detalles Bibliográficos
Autores principales: Aebischer, Kathrin, Ernst, Matthias
Formato: Online Artículo Texto
Lenguaje:English
Publicado: The Royal Society of Chemistry 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10155489/
https://www.ncbi.nlm.nih.gov/pubmed/36987593
http://dx.doi.org/10.1039/d3cp00414g