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X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films

Differential deposition by DC magnetron sputtering was applied to correct for figure errors of X-ray mirrors to be deployed on low-emittance synchrotron beamlines. During the deposition process, the mirrors were moved in front of a beam-defining aperture and the required velocity profile was calcula...

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Autores principales: Bras, Patrice, Morawe, Christian, Labouré, Sylvain, Perrin, François, Vivo, Amparo, Barrett, Raymond
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10325008/
https://www.ncbi.nlm.nih.gov/pubmed/37255023
http://dx.doi.org/10.1107/S1600577523003697
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author Bras, Patrice
Morawe, Christian
Labouré, Sylvain
Perrin, François
Vivo, Amparo
Barrett, Raymond
author_facet Bras, Patrice
Morawe, Christian
Labouré, Sylvain
Perrin, François
Vivo, Amparo
Barrett, Raymond
author_sort Bras, Patrice
collection PubMed
description Differential deposition by DC magnetron sputtering was applied to correct for figure errors of X-ray mirrors to be deployed on low-emittance synchrotron beamlines. During the deposition process, the mirrors were moved in front of a beam-defining aperture and the required velocity profile was calculated using a deconvolution algorithm. The surface figure was characterized using conventional off-line visible-light metrology instrumentation (long trace profiler and Fizeau interferometer) before and after the deposition. WSi(2) was revealed to be a promising candidate material since it conserves the initial substrate surface roughness and limits the film stress to acceptable levels. On a 300 mm-long flat Si mirror the average height errors were reduced by a factor of 20 down to 0.2 nm root mean square. This result shows the suitability of WSi(2) for differential deposition. Potential promising applications include the upgrade of affordable, average-quality substrates to the standards of modern synchrotron beamlines.
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spelling pubmed-103250082023-07-07 X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films Bras, Patrice Morawe, Christian Labouré, Sylvain Perrin, François Vivo, Amparo Barrett, Raymond J Synchrotron Radiat Research Papers Differential deposition by DC magnetron sputtering was applied to correct for figure errors of X-ray mirrors to be deployed on low-emittance synchrotron beamlines. During the deposition process, the mirrors were moved in front of a beam-defining aperture and the required velocity profile was calculated using a deconvolution algorithm. The surface figure was characterized using conventional off-line visible-light metrology instrumentation (long trace profiler and Fizeau interferometer) before and after the deposition. WSi(2) was revealed to be a promising candidate material since it conserves the initial substrate surface roughness and limits the film stress to acceptable levels. On a 300 mm-long flat Si mirror the average height errors were reduced by a factor of 20 down to 0.2 nm root mean square. This result shows the suitability of WSi(2) for differential deposition. Potential promising applications include the upgrade of affordable, average-quality substrates to the standards of modern synchrotron beamlines. International Union of Crystallography 2023-05-30 /pmc/articles/PMC10325008/ /pubmed/37255023 http://dx.doi.org/10.1107/S1600577523003697 Text en © Patrice Bras et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Bras, Patrice
Morawe, Christian
Labouré, Sylvain
Perrin, François
Vivo, Amparo
Barrett, Raymond
X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
title X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
title_full X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
title_fullStr X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
title_full_unstemmed X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
title_short X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
title_sort x-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin wsi(2) films
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10325008/
https://www.ncbi.nlm.nih.gov/pubmed/37255023
http://dx.doi.org/10.1107/S1600577523003697
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