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X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films
Differential deposition by DC magnetron sputtering was applied to correct for figure errors of X-ray mirrors to be deployed on low-emittance synchrotron beamlines. During the deposition process, the mirrors were moved in front of a beam-defining aperture and the required velocity profile was calcula...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10325008/ https://www.ncbi.nlm.nih.gov/pubmed/37255023 http://dx.doi.org/10.1107/S1600577523003697 |
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author | Bras, Patrice Morawe, Christian Labouré, Sylvain Perrin, François Vivo, Amparo Barrett, Raymond |
author_facet | Bras, Patrice Morawe, Christian Labouré, Sylvain Perrin, François Vivo, Amparo Barrett, Raymond |
author_sort | Bras, Patrice |
collection | PubMed |
description | Differential deposition by DC magnetron sputtering was applied to correct for figure errors of X-ray mirrors to be deployed on low-emittance synchrotron beamlines. During the deposition process, the mirrors were moved in front of a beam-defining aperture and the required velocity profile was calculated using a deconvolution algorithm. The surface figure was characterized using conventional off-line visible-light metrology instrumentation (long trace profiler and Fizeau interferometer) before and after the deposition. WSi(2) was revealed to be a promising candidate material since it conserves the initial substrate surface roughness and limits the film stress to acceptable levels. On a 300 mm-long flat Si mirror the average height errors were reduced by a factor of 20 down to 0.2 nm root mean square. This result shows the suitability of WSi(2) for differential deposition. Potential promising applications include the upgrade of affordable, average-quality substrates to the standards of modern synchrotron beamlines. |
format | Online Article Text |
id | pubmed-10325008 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-103250082023-07-07 X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films Bras, Patrice Morawe, Christian Labouré, Sylvain Perrin, François Vivo, Amparo Barrett, Raymond J Synchrotron Radiat Research Papers Differential deposition by DC magnetron sputtering was applied to correct for figure errors of X-ray mirrors to be deployed on low-emittance synchrotron beamlines. During the deposition process, the mirrors were moved in front of a beam-defining aperture and the required velocity profile was calculated using a deconvolution algorithm. The surface figure was characterized using conventional off-line visible-light metrology instrumentation (long trace profiler and Fizeau interferometer) before and after the deposition. WSi(2) was revealed to be a promising candidate material since it conserves the initial substrate surface roughness and limits the film stress to acceptable levels. On a 300 mm-long flat Si mirror the average height errors were reduced by a factor of 20 down to 0.2 nm root mean square. This result shows the suitability of WSi(2) for differential deposition. Potential promising applications include the upgrade of affordable, average-quality substrates to the standards of modern synchrotron beamlines. International Union of Crystallography 2023-05-30 /pmc/articles/PMC10325008/ /pubmed/37255023 http://dx.doi.org/10.1107/S1600577523003697 Text en © Patrice Bras et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Bras, Patrice Morawe, Christian Labouré, Sylvain Perrin, François Vivo, Amparo Barrett, Raymond X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films |
title | X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films |
title_full | X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films |
title_fullStr | X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films |
title_full_unstemmed | X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films |
title_short | X-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin WSi(2) films |
title_sort | x-ray mirrors with sub-nanometre figure errors obtained by differential deposition of thin wsi(2) films |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10325008/ https://www.ncbi.nlm.nih.gov/pubmed/37255023 http://dx.doi.org/10.1107/S1600577523003697 |
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