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Improved 2-pyridyl reductive homocoupling reaction using biorenewable solvent Cyrene™ (dihydrolevoglucosenone)

The synthesis of 5,5′-bis(trifluoromethyl)-2,2′-bipyridine using 2-bromo-5-(trifluoromethyl) pyridine was achieved at 50 °C using palladium acetate, tetrabutylammonium iodide (TBAI), potassium carbonate, and isopropanol in Cyrene™ (dihydrolevoglucosenone), a bio-renewable “green” solvent formed by a...

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Detalles Bibliográficos
Autores principales: Webb, Daniel A., Alsudani, Zeid, Xu, Guolin, Gao, Peng, Arnold, Leggy A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: RSC 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10484179/
https://www.ncbi.nlm.nih.gov/pubmed/38013944
http://dx.doi.org/10.1039/d3su00005b