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Origin of the residual line width under frequency-switched Lee–Goldburg decoupling in MAS solid-state NMR

Homonuclear decoupling sequences in solid-state nuclear magnetic resonance (NMR) under magic-angle spinning (MAS) show experimentally significantly larger residual line width than expected from Floquet theory to second order. We present an in-depth theoretical and experimental analysis of the origin...

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Detalles Bibliográficos
Autores principales: Hellwagner, Johannes, Grunwald, Liam, Ochsner, Manuel, Zindel, Daniel, Meier, Beat H., Ernst, Matthias
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Copernicus GmbH 2020
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10500695/
https://www.ncbi.nlm.nih.gov/pubmed/37904890
http://dx.doi.org/10.5194/mr-1-13-2020