Cargando…
Origin of the residual line width under frequency-switched Lee–Goldburg decoupling in MAS solid-state NMR
Homonuclear decoupling sequences in solid-state nuclear magnetic resonance (NMR) under magic-angle spinning (MAS) show experimentally significantly larger residual line width than expected from Floquet theory to second order. We present an in-depth theoretical and experimental analysis of the origin...
Autores principales: | Hellwagner, Johannes, Grunwald, Liam, Ochsner, Manuel, Zindel, Daniel, Meier, Beat H., Ernst, Matthias |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Copernicus GmbH
2020
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10500695/ https://www.ncbi.nlm.nih.gov/pubmed/37904890 http://dx.doi.org/10.5194/mr-1-13-2020 |
Ejemplares similares
-
Residual proton line width under refocused frequency-switched Lee-Goldburg decoupling in MAS NMR
por: Aebischer, Kathrin, et al.
Publicado: (2023) -
Residual dipolar line width in magic-angle spinning proton solid-state NMR
por: Chávez, Matías, et al.
Publicado: (2021) -
Spinning faster: protein NMR at MAS frequencies up to 126 kHz
por: Penzel, Susanne, et al.
Publicado: (2019) -
Rationalising Heteronuclear Decoupling in Refocussing Applications of Solid‐State NMR Spectroscopy
por: Frantsuzov, Ilya, et al.
Publicado: (2017) -
Homonuclear Decoupling in (1)H NMR of Solids by Remote Correlation
por: Moutzouri, Pinelopi, et al.
Publicado: (2020)