Protocol for (E)-selective semihydrogenation of alkynes using iridium-based catalyst

In this protocol, we describe highly (E)-selective alkyne semihydrogenation employing commercially available iridium complex and a bidentate phosphine ligand. We provide steps for (E)-stilbene synthesis, remaining formic acid neutralization, and determination of the (Z)/(E) ratio using gas chromatog...

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Detalles Bibliográficos
Autores principales: Kusy, Rafał, Grela, Karol
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Protocol
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10519852/
https://www.ncbi.nlm.nih.gov/pubmed/37733598
http://dx.doi.org/10.1016/j.xpro.2023.102579

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10519852/
https://www.ncbi.nlm.nih.gov/pubmed/37733598
http://dx.doi.org/10.1016/j.xpro.2023.102579

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