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7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate
The title compound, C(30)H(26)Br(2)O(4)·C(2)H(5)OH, was synthesized from the reaction between 5-bromosalicybenzaldehyde and 5,5-dimethyl-1,3-cyclohexanedione. The crystal packing is stabilized by intermolecular O—H⋯O hydrogen bonds and C—H⋯O interactions.
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970291/ https://www.ncbi.nlm.nih.gov/pubmed/21577903 http://dx.doi.org/10.1107/S1600536809035922 |
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author | Lian, Chaomei Lu, Pingping Zhu, Yulin |
author_facet | Lian, Chaomei Lu, Pingping Zhu, Yulin |
author_sort | Lian, Chaomei |
collection | PubMed |
description | The title compound, C(30)H(26)Br(2)O(4)·C(2)H(5)OH, was synthesized from the reaction between 5-bromosalicybenzaldehyde and 5,5-dimethyl-1,3-cyclohexanedione. The crystal packing is stabilized by intermolecular O—H⋯O hydrogen bonds and C—H⋯O interactions. |
format | Text |
id | pubmed-2970291 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29702912010-12-30 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate Lian, Chaomei Lu, Pingping Zhu, Yulin Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(30)H(26)Br(2)O(4)·C(2)H(5)OH, was synthesized from the reaction between 5-bromosalicybenzaldehyde and 5,5-dimethyl-1,3-cyclohexanedione. The crystal packing is stabilized by intermolecular O—H⋯O hydrogen bonds and C—H⋯O interactions. International Union of Crystallography 2009-09-12 /pmc/articles/PMC2970291/ /pubmed/21577903 http://dx.doi.org/10.1107/S1600536809035922 Text en © Lian et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Lian, Chaomei Lu, Pingping Zhu, Yulin 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate |
title | 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate |
title_full | 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate |
title_fullStr | 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate |
title_full_unstemmed | 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate |
title_short | 7-Bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1H-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4H)-one ethanol solvate |
title_sort | 7-bromo-4-(7-bromo-3,3-dimethyl-1-oxo-2,3,4,9-tetrahydro-1h-xanthen-9-yl)-3,3-dimethyl-2,3-dihydroxanthen-1(4h)-one ethanol solvate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970291/ https://www.ncbi.nlm.nih.gov/pubmed/21577903 http://dx.doi.org/10.1107/S1600536809035922 |
work_keys_str_mv | AT lianchaomei 7bromo47bromo33dimethyl1oxo2349tetrahydro1hxanthen9yl33dimethyl23dihydroxanthen14honeethanolsolvate AT lupingping 7bromo47bromo33dimethyl1oxo2349tetrahydro1hxanthen9yl33dimethyl23dihydroxanthen14honeethanolsolvate AT zhuyulin 7bromo47bromo33dimethyl1oxo2349tetrahydro1hxanthen9yl33dimethyl23dihydroxanthen14honeethanolsolvate |