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Determining the structure of a benzene7.2-silicalite-1 zeolite using a single-crystal X-ray method
A simple method for preparing orthorhombic single crystals of benzene-silicalite-1 was developed. A silicalite-1 crystal was pressed with a weight of 2 g along the +c and −c crystallographic axes while the temperature was increased to 473 K. The temperature was then slowly reduced to 313 K, and thes...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2011
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3222141/ https://www.ncbi.nlm.nih.gov/pubmed/22101540 http://dx.doi.org/10.1107/S0108768111038560 |