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Solid-state MAS NMR, TEM, and TGA studies of structural hydroxyl groups and water in nanocrystalline apatites prepared by dry milling

A series of nanocrystalline calcium hydroxyapatites was prepared by dry milling and characterized using proton and (31)P MAS NMR, TEM, and TGA methods. The samples contained stubby rod-shaped crystals, which length and width varied in the 130–30 and 95–20 nm ranges, respectively. It was confirmed th...

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Detalles Bibliográficos
Autores principales: Pajchel, Lukasz, Kolodziejski, Waclaw
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer Netherlands 2013
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3751289/
https://www.ncbi.nlm.nih.gov/pubmed/23990754
http://dx.doi.org/10.1007/s11051-013-1868-y