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Crystal structure of ethyl 2-(di­eth­oxy­phosphor­yl)-2-(2,3,4-tri­meth­oxy­phen­yl)acetate

The title compound, C(17)H(27)O(8)P, was prepared by Michaelis–Arbuzov reaction of ethyl 2-bromo-2-(2,3,4-tri­meth­oxy­phen­yl)acetate and triethyl phosphite. Such compounds rarely crystallize, but single crystals were recovered after the initial oil was left for approximately 10 years. The bond ang...

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Detalles Bibliográficos
Autores principales: Schubert, Moritz, Schollmeyer, Dieter, Waldvogel, Siegfried R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186086/
https://www.ncbi.nlm.nih.gov/pubmed/25309241
http://dx.doi.org/10.1107/S1600536814015803