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Crystal structure of ethyl 2-(diethoxyphosphoryl)-2-(2,3,4-trimethoxyphenyl)acetate
The title compound, C(17)H(27)O(8)P, was prepared by Michaelis–Arbuzov reaction of ethyl 2-bromo-2-(2,3,4-trimethoxyphenyl)acetate and triethyl phosphite. Such compounds rarely crystallize, but single crystals were recovered after the initial oil was left for approximately 10 years. The bond ang...
Autores principales: | Schubert, Moritz, Schollmeyer, Dieter, Waldvogel, Siegfried R. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2014
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186086/ https://www.ncbi.nlm.nih.gov/pubmed/25309241 http://dx.doi.org/10.1107/S1600536814015803 |
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