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Comparison of crystal structures of 4-(benzo[b]thio­phen-2-yl)-5-(3,4,5-tri­meth­oxy­phen­yl)-2H-1,2,3-triazole and 4-(benzo[b]thio­phen-2-yl)-2-methyl-5-(3,4,5-tri­meth­oxy­phen­yl)-2H-1,2,3-triazole

The title compound, C(19)H(17)N(3)O(3)S (I), was prepared by a [3 + 2]cyclo­addition azide condensation reaction using sodium azide and l-proline as a Lewis base catalyst. N-Methyl­ation of compound (I) using CH(3)I gave compound (II), C(20)H(19)N(3)O(3)S. The benzo­thio­phene ring systems in (I) an...

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Detalles Bibliográficos
Autores principales: Penthala, Narsimha Reddy, Madadi, Nikhil Reddy, Bommagani, Shobanbabu, Parkin, Sean, Crooks, Peter A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4257340/
https://www.ncbi.nlm.nih.gov/pubmed/25484755
http://dx.doi.org/10.1107/S1600536814023095