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Crystal structure of rac-(3a’R,9a’R)-3a’-(indol-3-yl)-1′,2′,3′,3a’,4′,9a’-hexa­hydro­spiro­[cyclo­pentane-1,9′-penta­leno[1,2-b]indole] p-xylene hemisolvate

The title compound, C(26)H(26)N(2)·0.5C(8)H(10), is the first reported characterized 2:2 product from acid-catalyzed condensation of indole with cyclo­penta­none and no other 2:2 products were observed. Recrystallization from p-xylene gave the title hemisolvate with the p-xylene mol­ecule located ab...

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Detalles Bibliográficos
Autores principales: Noland, Wayland E., Worth, Matthew A., Schneerer, Andrew K., Paal, Courtney L., Tritch, Kenneth J.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420065/
https://www.ncbi.nlm.nih.gov/pubmed/25995869
http://dx.doi.org/10.1107/S2056989015007422