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Crystal structure of rac-(3a’R,9a’R)-3a’-(indol-3-yl)-1′,2′,3′,3a’,4′,9a’-hexahydrospiro[cyclopentane-1,9′-pentaleno[1,2-b]indole] p-xylene hemisolvate
The title compound, C(26)H(26)N(2)·0.5C(8)H(10), is the first reported characterized 2:2 product from acid-catalyzed condensation of indole with cyclopentanone and no other 2:2 products were observed. Recrystallization from p-xylene gave the title hemisolvate with the p-xylene molecule located ab...
Autores principales: | Noland, Wayland E., Worth, Matthew A., Schneerer, Andrew K., Paal, Courtney L., Tritch, Kenneth J. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4420065/ https://www.ncbi.nlm.nih.gov/pubmed/25995869 http://dx.doi.org/10.1107/S2056989015007422 |
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