Isolation of 3-amino-4-nitro­benzyl acetate: evidence of an undisclosed impurity in 5-amino-2-nitro­benzoic acid

Yellow crystals of the title compound 3-amino-4-nitro­benzyl acetate, C(9)H(10)N(2)O(4), were isolated from the reaction of acetic anhydride with (5-amino-2-nitro­phen­yl)methanol, prepared from reduction of commerically available 5-amino-2-nitro­benzoic acid with borane–THF. The mol­ecule is essent...

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Detalles Bibliográficos
Autores principales: Quillian, Brandon, Hendricks, Jordan, Trivitayakhun, Matthew, Padgett, Clifford W.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4459301/
https://www.ncbi.nlm.nih.gov/pubmed/26090132
http://dx.doi.org/10.1107/S2056989015008750

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4459301/
https://www.ncbi.nlm.nih.gov/pubmed/26090132
http://dx.doi.org/10.1107/S2056989015008750

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