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Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning

Screw dislocations play an important role in materials' mechanical, electrical and optical properties. However, imaging the atomic displacements in screw dislocations remains challenging. Although advanced electron microscopy techniques have allowed atomic-scale characterization of edge disloca...

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Autores principales: Yang, H., Lozano, J. G., Pennycook, T. J., Jones, L., Hirsch, P. B., Nellist, P. D.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Pub. Group 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4468905/
https://www.ncbi.nlm.nih.gov/pubmed/26041257
http://dx.doi.org/10.1038/ncomms8266
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author Yang, H.
Lozano, J. G.
Pennycook, T. J.
Jones, L.
Hirsch, P. B.
Nellist, P. D.
author_facet Yang, H.
Lozano, J. G.
Pennycook, T. J.
Jones, L.
Hirsch, P. B.
Nellist, P. D.
author_sort Yang, H.
collection PubMed
description Screw dislocations play an important role in materials' mechanical, electrical and optical properties. However, imaging the atomic displacements in screw dislocations remains challenging. Although advanced electron microscopy techniques have allowed atomic-scale characterization of edge dislocations from the conventional end-on view, for screw dislocations, the atoms are predominantly displaced parallel to the dislocation line, and therefore the screw displacements are parallel to the electron beam and become invisible when viewed end-on. Here we show that screw displacements can be imaged directly with the dislocation lying in a plane transverse to the electron beam by optical sectioning using annular dark field imaging in a scanning transmission electron microscope. Applying this technique to a mixed [a+c] dislocation in GaN allows direct imaging of a screw dissociation with a 1.65-nm dissociation distance, thereby demonstrating a new method for characterizing dislocation core structures.
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spelling pubmed-44689052015-06-30 Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning Yang, H. Lozano, J. G. Pennycook, T. J. Jones, L. Hirsch, P. B. Nellist, P. D. Nat Commun Article Screw dislocations play an important role in materials' mechanical, electrical and optical properties. However, imaging the atomic displacements in screw dislocations remains challenging. Although advanced electron microscopy techniques have allowed atomic-scale characterization of edge dislocations from the conventional end-on view, for screw dislocations, the atoms are predominantly displaced parallel to the dislocation line, and therefore the screw displacements are parallel to the electron beam and become invisible when viewed end-on. Here we show that screw displacements can be imaged directly with the dislocation lying in a plane transverse to the electron beam by optical sectioning using annular dark field imaging in a scanning transmission electron microscope. Applying this technique to a mixed [a+c] dislocation in GaN allows direct imaging of a screw dissociation with a 1.65-nm dissociation distance, thereby demonstrating a new method for characterizing dislocation core structures. Nature Pub. Group 2015-06-04 /pmc/articles/PMC4468905/ /pubmed/26041257 http://dx.doi.org/10.1038/ncomms8266 Text en Copyright © 2015, Nature Publishing Group, a division of Macmillan Publishers Limited. All Rights Reserved. http://creativecommons.org/licenses/by/4.0/ This work is licensed under a Creative Commons Attribution 4.0 International License. The images or other third party material in this article are included in the article's Creative Commons license, unless indicated otherwise in the credit line; if the material is not included under the Creative Commons license, users will need to obtain permission from the license holder to reproduce the material. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/
spellingShingle Article
Yang, H.
Lozano, J. G.
Pennycook, T. J.
Jones, L.
Hirsch, P. B.
Nellist, P. D.
Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
title Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
title_full Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
title_fullStr Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
title_full_unstemmed Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
title_short Imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
title_sort imaging screw dislocations at atomic resolution by aberration-corrected electron optical sectioning
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4468905/
https://www.ncbi.nlm.nih.gov/pubmed/26041257
http://dx.doi.org/10.1038/ncomms8266
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