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High resolution 4D HPCH experiment for sequential assignment of (13)C-labeled RNAs via phosphodiester backbone

The three-dimensional structure determination of RNAs by NMR spectroscopy requires sequential resonance assignment, often hampered by assignment ambiguities and limited dispersion of (1)H and (13)C chemical shifts, especially of C4′/H4′. Here we present a novel through-bond 4D HPCH NMR experiment in...

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Detalles Bibliográficos
Autores principales:	Saxena, Saurabh, Stanek, Jan, Cevec, Mirko, Plavec, Janez, Koźmiński, Wiktor
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Springer Netherlands 2015
Materias:	Article
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4642592/ https://www.ncbi.nlm.nih.gov/pubmed/26409925 http://dx.doi.org/10.1007/s10858-015-9989-5

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