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Crystal structure of rac-3-[2,3-bis­(phenyl­sulfan­yl)-3H-indol-3-yl]propanoic acid

The title compound, C(23)H(19)NO(2)S(2), was obtained as an unexpected regioisomer from an attempted synthesis of an inter­mediate for a substituent-effect study on ergot alkaloids. This is the first report of a 1H-indole mono­thio­ating at the 2- and 3-positions to give a 3H-indole. In the crystal,...

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Detalles Bibliográficos
Autores principales: Noland, Wayland E., Brown, Christopher D., Bisel, Amanda M., Schneerer, Andrew K., Tritch, Kenneth J.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4645081/
https://www.ncbi.nlm.nih.gov/pubmed/26594523
http://dx.doi.org/10.1107/S2056989015020241