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(13)C SPE MAS measurement of ligand concentration in compressible chromatographic beads

A method for measuring the ligand concentration in heterogeneous materials like chromatography media is described. In this method, (13)C single pulse excitation magic angle spinning NMR experiment with broadband (1)H decoupling is used to determine the peak integrals for a butyl ligand in the spectr...

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Detalles Bibliográficos
Autores principales: Elwinger, Fredrik, Dvinskikh, Sergey V., Furó, István
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2015
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4832835/
https://www.ncbi.nlm.nih.gov/pubmed/26053054
http://dx.doi.org/10.1002/mrc.4257