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(13)C SPE MAS measurement of ligand concentration in compressible chromatographic beads
A method for measuring the ligand concentration in heterogeneous materials like chromatography media is described. In this method, (13)C single pulse excitation magic angle spinning NMR experiment with broadband (1)H decoupling is used to determine the peak integrals for a butyl ligand in the spectr...
Autores principales: | Elwinger, Fredrik, Dvinskikh, Sergey V., Furó, István |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
John Wiley and Sons Inc.
2015
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC4832835/ https://www.ncbi.nlm.nih.gov/pubmed/26053054 http://dx.doi.org/10.1002/mrc.4257 |
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