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A new protocol for the synthesis of 4,7,12,15-tetrachloro[2.2]paracyclophane
We report a green and convenient protocol to prepare 4,7,12,15-tetrachloro[2.2]paracyclophane, the precursor of parylene D, from 2,5-dichloro-p-xylene. In the first bromination step, with H(2)O(2)–HBr as a bromide source, this procedure becomes organic-waste-free and organic-solvent-free and can app...
| Autores principales: | , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
Beilstein-Institut
2016
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5238561/ https://www.ncbi.nlm.nih.gov/pubmed/28144311 http://dx.doi.org/10.3762/bjoc.12.237 |