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Preparation of High Purity Trimethylborane1

The preparation of high-purity trimethylborane is described. Impurities were removed by fractionation of the ammonia adduct, NH(3):B(CH3)(3). Mass spectrometric analyses were used during the fractionation to determine these impurities. After purification of the B (CH(3))(3) in the form of its ammoni...

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Detalles Bibliográficos
Autores principales: Ross, Gaylon S., Enagonio, Delmo, Hewitt, Clifford A., Glasgow, Augustus R.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: [Gaithersburg, MD] : U.S. Dept. of Commerce, National Institute of Standards and Technology 1962
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5327742/
http://dx.doi.org/10.6028/jres.066A.006