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Preparation of High Purity Trimethylborane1
The preparation of high-purity trimethylborane is described. Impurities were removed by fractionation of the ammonia adduct, NH(3):B(CH3)(3). Mass spectrometric analyses were used during the fractionation to determine these impurities. After purification of the B (CH(3))(3) in the form of its ammoni...
Autores principales: | Ross, Gaylon S., Enagonio, Delmo, Hewitt, Clifford A., Glasgow, Augustus R. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
[Gaithersburg, MD] : U.S. Dept. of Commerce, National Institute of Standards and Technology
1962
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5327742/ http://dx.doi.org/10.6028/jres.066A.006 |
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