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Crystal structure of methyl (4R)-4-(4-meth­oxy­benzo­yl)-4-{[(1R)-1-phenyl­eth­yl]carbamo­yl}butano­ate

The title compound, C(22)H(25)NO(5), was prepared by CAN [cerium(IV) ammonium nitrate] oxidation of the corresponding β-lactam. The dihedral angle between the benzene rings is 13.3 (4)° and the C—N—C(=O)—C torsion angle is 176.1 (6)°. In the crystal, amide-C(4) N—H⋯O and reinforcing C—H⋯O hydrogen b...

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Detalles Bibliográficos
Autores principales: Manchado, Alejandro, Salgado, Mateo M., Vicente, Álvaro, Díez, David, Sanz, Francisca, Garrido, Narciso M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5382608/
https://www.ncbi.nlm.nih.gov/pubmed/28435707
http://dx.doi.org/10.1107/S2056989017003607