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Rationalising Heteronuclear Decoupling in Refocussing Applications of Solid‐State NMR Spectroscopy

Factors affecting the performance of (1)H heteronuclear decoupling sequences for magic‐angle spinning (MAS) NMR spectroscopy of organic solids are explored, as observed by time constants for the decay of nuclear magnetisation under a spin‐echo ([Formula: see text] ). By using a common protocol over...

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Detalles Bibliográficos
Autores principales: Frantsuzov, Ilya, Vasa, Suresh K., Ernst, Matthias, Brown, Steven P., Zorin, Vadim, Kentgens, Arno P. M., Hodgkinson, Paul
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5396389/
https://www.ncbi.nlm.nih.gov/pubmed/28111874
http://dx.doi.org/10.1002/cphc.201601003