Limits of Resolution and Sensitivity of Proton Detected MAS Solid-State NMR Experiments at 111 kHz in Deuterated and Protonated Proteins

MAS solid-state NMR is capable of determining structures of protonated solid proteins using proton-detected experiments. These experiments are performed at MAS rotation frequency of around 110 kHz, employing 0.5 mg of material. Here, we compare (1)H, (13)C correlation spectra obtained from protonate...

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Detalles Bibliográficos
Autores principales: Xue, Kai, Sarkar, Riddhiman, Motz, Carina, Asami, Sam, Camargo, Diana C. Rodriguez, Decker, Venita, Wegner, Sebastian, Tosner, Zdenek, Reif, Bernd
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2017
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5547042/
https://www.ncbi.nlm.nih.gov/pubmed/28785098
http://dx.doi.org/10.1038/s41598-017-07253-1

Internet

https://www.ncbi.nlm.nih.gov/pmc/articles/PMC5547042/
https://www.ncbi.nlm.nih.gov/pubmed/28785098
http://dx.doi.org/10.1038/s41598-017-07253-1

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